Benzenamine, 4-(4-chlorophenoxy)-3-nitro-

Base Information

• Chemical Name: Benzenamine, 4-(4-chlorophenoxy)-3-nitro-
• CAS No.: 83660-66-6
• Molecular Formula: C12H9ClN2O3
• Molecular Weight: 264.668
• Mol file: 83660-66-6.mol

Synonyms:

Chemical Property of Benzenamine, 4-(4-chlorophenoxy)-3-nitro-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 4-(4-chlorophenoxy)-3-nitro-

There total 1 articles about Benzenamine, 4-(4-chlorophenoxy)-3-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Fluoro-3-nitroaniline (364-76-1) + 4-chloro-phenol (106-48-9,82344-39-6) → 4-(4-chlorophenoxy)-3-nitroaniline (83660-66-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 3h;

Reference yield:

4-(4-chlorophenoxy)-3-nitroaniline (83660-66-6) → 4-(4-chlorophenoxy)-3-nitrophenylhydrazine (359714-71-9)

Guidance literature:

4-(4-chlorophenoxy)-3-nitroaniline; With hydrogenchloride; sodium nitrite; In ethanol; water; at 0 ℃; for 1h;

With hydrogenchloride; tin(ll) chloride; In ethanol; water;

Reference yield:

4-(4-chlorophenoxy)-3-nitroaniline (83660-66-6) + sodium nitrite (7632-00-0) → 4-(4-chlorophenoxy)-3-nitrophenylhydrazine (359714-71-9)

Guidance literature:

4-(4-chlorophenoxy)-3-nitroaniline; sodium nitrite; With hydrogenchloride; In ethanol; water; at 0 ℃; for 1h;

With tin(ll) chloride;

upstream raw materials:

4-Fluoro-3-nitroaniline

4-chloro-phenol

Downstream raw materials:

4-(4-chlorophenoxy)-3-nitrophenylhydrazine

Refernces

• 1、 -. "Substituted 3-phenyl-5-alkoxy-1,3,4-oxadiazol-2-ones, their preparation and their use as pharmaceuticals". Example 7. . Retrieved 2008/06/13.