2-(Tribromomethyl)quinoxaline

Base Information

Chemical Name:2-(Tribromomethyl)quinoxaline
CAS No.:7251-36-7
Molecular Formula:C9H5Br3N2
Molecular Weight:380.8614
Hs Code.:2933990090
European Community (EC) Number:654-366-7
NSC Number:71311
DSSTox Substance ID:DTXSID00222826
Nikkaji Number:J48.376A
Wikidata:Q83101170
Mol file:7251-36-7.mol

Synonyms:2-(Tribromomethyl)quinoxaline;2-Tribromomethylquinoxaline;Quinoxaline, 2-(tribromomethyl)-;7251-36-7;NSC 71311;BRN 0157314;NSC71311;NCIOpen2_008565;4-23-00-01253 (Beilstein Handbook Reference);SCHEMBL5720367;WLN: T66 BN ENJ CXEEE;DTXSID00222826;VCCOPRMZNNMFLI-UHFFFAOYSA-N;NSC-71311;AKOS024429114

Suppliers and Price of 2-(Tribromomethyl)quinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-TRIBROMOMETHYLQUINOXALINE Aldrich
250mg
$ 144.00

Total 4 raw suppliers

Chemical Property of 2-(Tribromomethyl)quinoxaline

Chemical Property:

Vapor Pressure:2.77E-05mmHg at 25°C
Boiling Point:368°Cat760mmHg
Flash Point:176.4°C
PSA：25.78000
Density:2.284g/cm³
LogP:3.92480
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:379.79824
Heavy Atom Count:14
Complexity:205

Purity/Quality:: 2-TRIBROMOMETHYLQUINOXALINE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)N=CC(=N2)C(Br)(Br)Br

Technology Process of 2-(Tribromomethyl)quinoxaline

There total 4 articles about 2-(Tribromomethyl)quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 7251-61-8
2-methylquinoxaline

: 54804-43-2
2-(bromomethyl)quinoxaline

: 32601-90-4
2-(dibromomethyl)quinoxaline

: 7251-36-7
2-(Tribromomethyl)quinoxaline

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 80 ℃; for 5h;
DOI:10.1039/b001296n

Reference yield:

: 7251-61-8
2-methylquinoxaline

: 7251-36-7
2-(Tribromomethyl)quinoxaline

Guidance literature:: With bromine; sodium acetate; acetic acid; at 70 ℃;

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 7251-36-7
2-(Tribromomethyl)quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium metabisulfite / H₂O / 0.17 h

1.2: 91 percent / H₂O / 18 h / 20 °C

2.1: 2 percent / NBS; benzoyl peroxide / CCl₄ / 5 h / 80 °C

With sodium disulfite; N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; water; 1.1: Addition / 1.2: Condensation / 2.1: Bromination;
DOI:10.1039/b001296n