4,1-Benzoxazepine-3-ethanethioamide, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-

Base Information

Chemical Name:4,1-Benzoxazepine-3-ethanethioamide, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-
CAS No.:839724-59-3
Molecular Formula:C26H31ClN2O6S
Molecular Weight:535.061
Hs Code.:

4,1-Benzoxazepine-3-ethanethioamide,
1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1,
2,3,5-tetrahydro-2-oxo-, (3R,5S)-

Synonyms:

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Chemical Property of 4,1-Benzoxazepine-3-ethanethioamide, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-

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Technology Process of 4,1-Benzoxazepine-3-ethanethioamide, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-

There total 1 articles about 4,1-Benzoxazepine-3-ethanethioamide, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 839724-58-2
3-[(3R,5S)-3-(2-amino-2-oxoethyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate

: 839724-59-3
3-[(3R,5S)-3-(2-amino-2-thioxoethyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate

Guidance literature:: 3-[(3R,5S)-3-(2-amino-2-oxoethyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate; With Lawessons reagent; In tetrahydrofuran; for 1h; Heating / reflux;

With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 - 30 ℃; for 0.5h;

Reference yield:

: 839724-59-3
3-[(3R,5S)-3-(2-amino-2-thioxoethyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate

: ethyl 2-{[(3R,5S)-1-[3-acetoxy-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-1,2,3,5-tetrahydro-4,1-benzoxazepin-3-yl]methyl}-1,3-thiazol-5-carboxylate

Guidance literature:: With acetic acid; In isopropyl alcohol; for 30.5h; Heating / reflux;

Reference yield:

: 35196-48-6
ethyl 2-hydrazino-2-oxoacetate

: 839724-59-3
3-[(3R,5S)-3-(2-amino-2-thioxoethyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate

: C₂₈H₃₃ClN₄O₇

Guidance literature:: 3-[(3R,5S)-3-(2-amino-2-thioxoethyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate; With methyl iodide; In ethanol; acetone;

ethyl 2-hydrazino-2-oxoacetate; In butan-1-ol; for 2h; Heating / reflux;