N-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]METHANESULFONAMIDE

Base Information

Chemical Name:N-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]METHANESULFONAMIDE
CAS No.:843646-66-2
Molecular Formula:C14H22BNO4S
Molecular Weight:311.21
Hs Code.:
Mol file:843646-66-2.mol

Synonyms:3-(methanesulfonylamino-methyl)-phenylboronic acid, pinacol ester;N-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-methanesulfonamide;

Suppliers and Price of N-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]METHANESULFONAMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-[[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL]METHYL]METHANESULFONAMIDE 95.00%
5MG
$ 500.61

Total 1 raw suppliers

Chemical Property of N-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]METHANESULFONAMIDE

Chemical Property:

PSA：73.01000
LogP:2.50670

Purity/Quality:: N-[[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL]METHYL]METHANESULFONAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]METHANESULFONAMIDE

There total 4 articles about N-[3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZYL]METHANESULFONAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 380430-65-9
(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride salt

: 124-63-0
methanesulfonyl chloride

: 843646-66-2
N-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]methanesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 88.0%

: N-(3-iodo-benzyl)-methanesulfonamide

: 73183-34-3
bis(pinacol)diborane

: 843646-66-2
N-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]methanesulfonamide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium acetate; In polyethylene glycol 600; at 90 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/aoc.1799

Reference yield: 72.58%

: 885681-65-2
N-(3-bromobenzyl)methanesulfonamide

: 73183-34-3
bis(pinacol)diborane

: 843646-66-2
N-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl]methanesulfonamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 90 ℃; for 4h;