1-(9H-fluoren-9-yl)propan-2-one

Base Information

• Chemical Name: 1-(9H-fluoren-9-yl)propan-2-one
• CAS No.: 2470-85-1
• Molecular Formula: C₁₆H₁₄O
• Molecular Weight: 222.287
• Mol file: 2470-85-1.mol

Synonyms:2-Propanone,1-fluoren-9-yl- (8CI); 2-Propanone, fluoren-9-yl- (7CI);1-(9H-Fluoren-9-yl)propan-2-one

Chemical Property of 1-(9H-fluoren-9-yl)propan-2-one

Chemical Property:

• Vapor Pressure: 8.1E-06mmHg at 25°C
• Boiling Point: 374.9°Cat760mmHg
• Flash Point: 192.7°C
• PSA: 17.07000
• Density: 1.114g/cm³
• LogP: 3.77800

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(9H-fluoren-9-yl)propan-2-one

There total 5 articles about 1-(9H-fluoren-9-yl)propan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

acetone (67-64-1) + 9-diazofluorenone (832-80-4) → 9-Acetonyl-fluoren (2470-85-1) + 6,6-dimethyldibenzofulvene oxide (81277-93-2)

Guidance literature:

Irradiation;

DOI:10.1021/ja00310a090

Reference yield:

9H-fluoren-9-yl bromide (1940-57-4) + acetone (67-64-1) → 9-Acetonyl-fluoren (2470-85-1)

Guidance literature:

With potassium hydroxide; In acetone;

DOI:10.1246/bcsj.35.408

Reference yield:

methyl magnesium iodide (917-64-6) + 9-fluorenylmethylcarbonyl chloride (40356-30-7) → 9-Acetonyl-fluoren (2470-85-1)

Guidance literature:

With cadmium(II) chloride;

DOI:10.1246/bcsj.50.258

upstream raw materials:

methyl magnesium iodide

9-fluorenylmethylcarbonyl chloride

9-(prop-2-ynyl)-9H-fluorene

9H-fluoren-9-yl bromide