(Chloromethyl)phenylphosphinic chloride

Base Information

Chemical Name:(Chloromethyl)phenylphosphinic chloride
CAS No.:40561-09-9
Molecular Formula:C7H7 Cl2 O P
Molecular Weight:209.012
Hs Code.:
NSC Number:138347
DSSTox Substance ID:DTXSID20300690
Nikkaji Number:J2.113.238A
Mol file:40561-09-9.mol

Synonyms:(chloromethyl)phenylphosphinic chloride;40561-09-9;NSC138347;SCHEMBL6572723;DTXSID20300690;NSC-138347;Phosphinic chloride, (chloromethyl)phenyl-;3-(2-Propenyl)-2-hydroxy-1,4-naphthoquinone

Suppliers and Price of (Chloromethyl)phenylphosphinic chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (Chloromethyl)phenylphosphinic chloride

Chemical Property:

Vapor Pressure:0.000163mmHg at 25°C
Boiling Point:341.1°Cat760mmHg
Flash Point:160.1°C
Density:1.34g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:207.9611572
Heavy Atom Count:11
Complexity:166

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=O)(CCl)Cl

Technology Process of (Chloromethyl)phenylphosphinic chloride

There total 6 articles about (Chloromethyl)phenylphosphinic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 61451-78-3
(hydroxymethyl)(phenyl)phosphinic acid

: 40561-09-9
phenyl(chloromethyl)phosphinic acid chloride

Guidance literature:: With thionyl chloride; at 80 ℃; for 10h;
DOI:10.1016/j.jorganchem.2004.11.035

Reference yield:

: 94971-13-8
Chlormethyl-phenyl-phosphinsaeure-anhydrid

: 40561-09-9
phenyl(chloromethyl)phosphinic acid chloride

Guidance literature:: With phosphorus pentachloride; In tetrachloromethane;
DOI:10.1021/ja01482a021

Reference yield:

: 1779-48-2
phenylphosphinic acid

: 40561-09-9
phenyl(chloromethyl)phosphinic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / H₂O / 20 h / 80 °C

2: 71 percent / SOCl₂ / 10 h / 80 °C

With hydrogenchloride; thionyl chloride; In water; 1: Abramov addition;
DOI:10.1016/j.jorganchem.2004.11.035