[(3S,4S,5R,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyphosphon ic acid

Base Information

• Chemical Name: [(3S,4S,5R,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyphosphon ic acid
• CAS No.: 63779-58-8
• Molecular Formula: C₆H₁₃O₉P
• Molecular Weight: 260.138

Synonyms:Mannopyranose,1-(dihydrogen phosphate), D- (8CI); D-Mannopyranose, 1-phosphate; Mannosephosphate; Mannosyl phosphate

Chemical Property of [(3S,4S,5R,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyphosphon ic acid

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of [(3S,4S,5R,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyphosphon ic acid

There total 86 articles about [(3S,4S,5R,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyphosphon ic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

D-Glucose (2280-44-6) → α-D-glucopyranosyl-1-phosphate (59-56-3,27251-84-9,63779-58-8,262856-84-8)

Guidance literature:

With phosphoric acid; methyloxirane; In pyridine; 1.) 30 min, 2.) 40 deg C, 1 h;

Reference yield: 69.0%

dibezylphosphoryl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (82300-58-1) → α-D-glucopyranosyl-1-phosphate (59-56-3,27251-84-9,63779-58-8,262856-84-8)

Guidance literature:

With hydrogen; palladium; In tetrahydrofuran; ethyl acetate; for 0.5h;

Reference yield:

adenosin 5'-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl diphosphate) (81347-80-0) → glucose 1-phosphate (59-56-3,2240-08-6,2255-14-3,2520-52-7,6799-01-5,10456-01-6,14048-34-1,15978-07-1,19993-19-2,20299-62-1,40591-51-3,62057-78-7,77280-79-6,78341-19-2,27251-84-9,63779-58-8,262856-84-8) + 5'-adenosine monophosphate (61-19-8,24937-83-5,67583-85-1)

Guidance literature:

With sodium hydroxide; In methanol; water; at 25 ℃; for 50h;

DOI:10.1016/S0008-6215(00)81017-4

upstream raw materials:

dibenzyl (2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl) phosphate

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

Dibenzyl(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)phosphat

Dibenzyl(β-D-glucopyranosyl)phosphat

Downstream raw materials:

β-D-glucopyranosyl

O-α-D-Glucopyranosyl-(1-3)-α,β-L-rhamnopyranose

alpha-D-glucopyranose

α-D-galactopyranosyl phosphate

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