2,2,4,4-Tetramethyl-6-(2-methyl-1-oxopropyl)-1,3,5-cyclohexanetrione

Base Information

• Chemical Name: 2,2,4,4-Tetramethyl-6-(2-methyl-1-oxopropyl)-1,3,5-cyclohexanetrione
• CAS No.: 22595-45-5
• Molecular Formula: C14H20 O4
• Molecular Weight: 252.31
• Hs Code.: 2914299000
• Mol file: 22595-45-5.mol

Synonyms:1,3,5-Cyclohexanetrione,6-isobutyryl-2,2,4,4-tetramethyl- (7CI,8CI); Flavesone

Chemical Property of 2,2,4,4-Tetramethyl-6-(2-methyl-1-oxopropyl)-1,3,5-cyclohexanetrione

Chemical Property:

• PSA: 68.28000
• LogP: 1.60100

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2,4,4-Tetramethyl-6-(2-methyl-1-oxopropyl)-1,3,5-cyclohexanetrione

There total 2 articles about 2,2,4,4-Tetramethyl-6-(2-methyl-1-oxopropyl)-1,3,5-cyclohexanetrione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phlorisobutyrophenone (35458-21-0) + methyl iodide (74-88-4) → 6-isobutyryl-2,2,4,4-tetramethylcyclohexane-1,3,5-trione (22595-45-5)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1039/c7sc04672c

Reference yield:

→ 6-isobutyryl-2,2,4,4-tetramethylcyclohexane-1,3,5-trione (22595-45-5)

Guidance literature:

Phlorisobutyrophenon, Methylierung; neben anderen Verbb.;

Reference yield: 91.0%

6-isobutyryl-2,2,4,4-tetramethylcyclohexane-1,3,5-trione (22595-45-5) → 2,2,4,4-tetramethyl-6-(2-methylpropylidene)-cyclohexane-1,3,5-trione (61565-12-6)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; at -78 ℃;

DOI:10.1039/c7sc04672c

upstream raw materials:

phlorisobutyrophenone

methyl iodide