Pentachloroacetophenone

Base Information

Chemical Name:Pentachloroacetophenone
CAS No.:25201-35-8
Deprecated CAS:114690-60-7
Molecular Formula:C8H3 Cl5 O
Molecular Weight:292.376
Hs Code.:
DSSTox Substance ID:DTXSID20921460
Nikkaji Number:J90.782K
Mol file:25201-35-8.mol

Synonyms:pentachloroacetophenone

Suppliers and Price of Pentachloroacetophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PENTACHLORO ACETOPHENONE 95.00%
5MG
$ 497.16

Total 5 raw suppliers

Chemical Property of Pentachloroacetophenone

Chemical Property:

Vapor Pressure:0.000565mmHg at 25°C
Melting Point:90°C
Boiling Point:342.8°Cat760mmHg
Flash Point:144.7°C
PSA：17.07000
Density:1.617g/cm³
LogP:5.15620
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:291.859703
Heavy Atom Count:14
Complexity:218

Purity/Quality:

99% ^*data from raw suppliers

PENTACHLORO ACETOPHENONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=C(C(=C(C(=C1Cl)Cl)Cl)Cl)Cl

Technology Process of Pentachloroacetophenone

There total 4 articles about Pentachloroacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65426-69-9
1-(2,3,4,5,6-Pentachlorophenyl)ethanol

: 25201-35-8
2',3',4',5',6'-pentachloroacetophenone

Guidance literature:: With chromium(VI) oxide; acetic acid;
DOI:10.1021/ja01192a020

Reference yield:

: 65426-67-7
acetic acid-(1-pentachlorophenyl-ethyl ester)

: 25201-35-8
2',3',4',5',6'-pentachloroacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: (basic hydrolysis)

2: K₂Cr₂O₇, aq. H₂SO₄

With potassium dichromate; sulfuric acid;
DOI:10.1021/ja01463a038

Reference yield:

: 118-74-1,67471-27-6
hexachlorobenzene

: 25201-35-8
2',3',4',5',6'-pentachloroacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.33 h

1.2: 52 percent / tetrahydrofuran; hexane / -78 - 20 °C

2.1: Na₂Cr₂O₇; H₂SO₄ / diethyl ether; H₂O

With n-butyllithium; sodium dichromate; sulfuric acid; In tetrahydrofuran; diethyl ether; hexane; water;
DOI:10.1007/s11172-005-0341-1