Silane, dichloro[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl]oxy](2-methyl phenyl)-

Base Information

Chemical Name:Silane, dichloro[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl]oxy](2-methyl phenyl)-
CAS No.:847787-57-9
Molecular Formula:C17H26Cl2OSi
Molecular Weight:345.384
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, dichloro[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl]oxy](2-methyl phenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Silane, dichloro[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl]oxy](2-methyl phenyl)-

There total 2 articles about Silane, dichloro[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl]oxy](2-methyl phenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 2216-51-5
(-)-menthol

: 13835-81-9
trichloro(2-methylphenyl)silane

: 847787-57-9
(-)-dichloro-[(1R,2S,5R)-menthyloxy]-(2-methylphenyl)silane

Guidance literature:: With urea; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1002/ejoc.200400622

Reference yield:

: 95-46-5
2-methylphenyl bromide

: 847787-57-9
(-)-dichloro-[(1R,2S,5R)-menthyloxy]-(2-methylphenyl)silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / diethyl ether / 1 h / Heating

1.2: 53 percent / SiCl₄ / diethyl ether / 2 h / 40 °C

2.1: 65 percent / urea / diethyl ether / 3 h / 20 °C

With magnesium; urea; In diethyl ether;
DOI:10.1002/ejoc.200400622