(NZ)-N-[2-amino-1-[4-(trifluoromethyl)phenyl]ethylidene]hydroxylamine

Base Information

Chemical Name:(NZ)-N-[2-amino-1-[4-(trifluoromethyl)phenyl]ethylidene]hydroxylamine
CAS No.:82585-42-0
Molecular Formula:C9H9 F3 N2 O
Molecular Weight:218.1758
Hs Code.:
NSC Number:335413
DSSTox Substance ID:DTXSID90422914

Synonyms:NSC335413;82585-42-0;DTXSID90422914;NSC-335413

Suppliers and Price of (NZ)-N-[2-amino-1-[4-(trifluoromethyl)phenyl]ethylidene]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (NZ)-N-[2-amino-1-[4-(trifluoromethyl)phenyl]ethylidene]hydroxylamine

Chemical Property:

Vapor Pressure:0.00105mmHg at 25°C
Boiling Point:289°Cat760mmHg
Flash Point:128.6°C
Density:1.34g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:218.06669740
Heavy Atom Count:15
Complexity:232

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=NO)CN)C(F)(F)F
Isomeric SMILES:C1=CC(=CC=C1/C(=N/O)/CN)C(F)(F)F

Technology Process of (NZ)-N-[2-amino-1-[4-(trifluoromethyl)phenyl]ethylidene]hydroxylamine

There total 1 articles about (NZ)-N-[2-amino-1-[4-(trifluoromethyl)phenyl]ethylidene]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82585-55-5
2-[2-[(E)-Hydroxyimino]-2-(4-trifluoromethyl-phenyl)-ethyl]-isoindole-1,3-dione

: 82585-42-0
2-Amino-1-(4-trifluoromethyl-phenyl)-ethanone oxime

Guidance literature:: With hydrazine; In ethanol; at 40 ℃; for 22h; Yield given;
DOI:10.1021/jm00351a008

Reference yield: 47.0%

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 82585-42-0
2-Amino-1-(4-trifluoromethyl-phenyl)-ethanone oxime

: 82585-71-5
{6-Amino-4-[2-[(Z)-hydroxyimino]-2-(4-trifluoromethyl-phenyl)-ethylamino]-5-nitro-pyridin-2-yl}-carbamic acid ethyl ester

Guidance literature:: With triethylamine; In ethanol; at 75 ℃; for 2h;
DOI:10.1021/jm00351a008

Reference yield:

: 82585-42-0
2-Amino-1-(4-trifluoromethyl-phenyl)-ethanone oxime

: 82586-03-6
[5-Amino-3-(4-trifluoromethyl-phenyl)-1,2-dihydro-pyrido[3,4-b]pyrazin-7-yl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / Et₃N / ethanol / 2 h / 75 °C

2: 31 percent / 1N aq. HCl / dioxane / 2 h / 60 °C

3: 56 percent / H₂ / Raney nickel / ethanol; dioxane / 48 h / 760 Torr / Heating

With hydrogenchloride; hydrogen; triethylamine; nickel; In 1,4-dioxane; ethanol;
DOI:10.1021/jm00351a008