1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihydro-, dihydrochloride

Base Information

Chemical Name:1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihydro-, dihydrochloride
CAS No.:130482-62-1
Molecular Formula:C₁₅H₂₃N₃O₂*2ClH
Molecular Weight:350.288
Hs Code.:
DSSTox Substance ID:DTXSID00926756
Mol file:130482-62-1.mol

Synonyms:130482-62-1;1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihydro-, dihydrochloride;Dichlorure N-(diethylamino-2 ethyl)dihydro-2,3 benzodioxinne-1,4 carboximidamide-2 [French];1,4-Benzodioxin-2-carboximidamide, 2,3-dihydro-N-(2-(diethylamino)ethyl)-, hydrochloride, hydrate (2:4:1);Dichlorure N-(diethylamino-2 ethyl)dihydro-2,3 benzodioxinne-1,4 carboximidamide-2;1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihyd ro-, dihydrochloride;N'-[2-(diethylamino)ethyl]-2,3-dihydro-1,4-benzodioxine-3-carboximidamide;dihydrochloride;DTXSID00926756;LSTXZYMUZGALQI-UHFFFAOYSA-N;LS-34553;N-[2-(Diethylamino)ethyl]-2,3-dihydro-1,4-benzodioxine-2-carboximidamide--hydrogen chloride (1/2)

Suppliers and Price of 1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihydro-, dihydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihydro-, dihydrochloride

Chemical Property:

Vapor Pressure:1.04E-06mmHg at 25°C
Boiling Point:403.1°Cat760mmHg
Flash Point:197.6°C
PSA：57.58000
Density:g/cm³
LogP:3.82970
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:349.1323824
Heavy Atom Count:22
Complexity:318

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CCN=C(C1COC2=CC=CC=C2O1)N.Cl.Cl

Technology Process of 1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihydro-, dihydrochloride

There total 4 articles about 1,4-Benzodioxin-2-carboximidamide, N-(2-(diethylamino)ethyl)-2,3-dihydro-, dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 85084-36-2
chlorure de dihydro-2,3 benzodioxinne-1,4 carboxamidinium-2

: 100-36-7
N,N-diethylethylenediamine

: 130482-62-1
dichlorure de N-(diethylammonio-2 ethyl) dihydro 2,3-benzodioxinne-1,4 carboxamidinium-2

Guidance literature:: In ethanol; for 3.75h; Heating;
DOI:10.1016/0223-5234(90)90002-K

Reference yield:

: 1008-92-0
2-cyano-1,4-benzodioxane

: 130482-62-1
dichlorure de N-(diethylammonio-2 ethyl) dihydro 2,3-benzodioxinne-1,4 carboxamidinium-2

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / methylate de sodium / 24 h / Ambient temperature

2: 97 percent / chlorure d'ammonium / ethanol / 3.5 h / Heating

3: 70 percent / ethanol / 3.75 h / Heating

With ammonium chloride; sodium methylate; In ethanol;
DOI:10.1016/0223-5234(90)90002-K

Reference yield:

: 96717-31-6
diethyl-2,3-dihydro-1,4-benzodioxine-2-carboximidate

: 130482-62-1
dichlorure de N-(diethylammonio-2 ethyl) dihydro 2,3-benzodioxinne-1,4 carboxamidinium-2

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / chlorure d'ammonium / ethanol / 3.5 h / Heating

2: 70 percent / ethanol / 3.75 h / Heating

With ammonium chloride; In ethanol;
DOI:10.1016/0223-5234(90)90002-K