Benzenecarboximidic acid, 4-[2-[[[[(4-methylphenyl)sulfonyl]amino]acetyl]amino]-3-(4-morpholinyl)-3 -oxopropyl]-, methyl ester, monohydrochloride

Base Information

Chemical Name:Benzenecarboximidic acid, 4-[2-[[[[(4-methylphenyl)sulfonyl]amino]acetyl]amino]-3-(4-morpholinyl)-3 -oxopropyl]-, methyl ester, monohydrochloride
CAS No.:84792-55-2
Molecular Formula:C24H30N4O6S.ClH
Molecular Weight:539.052
Hs Code.:

Benzenecarboximidic acid,
4-[2-[[[[(4-methylphenyl)sulfonyl]amino]acetyl]amino]-3-(4-morpholinyl)-3
-oxopropyl]-, methyl ester, monohydrochloride

Synonyms:

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Chemical Property of Benzenecarboximidic acid, 4-[2-[[[[(4-methylphenyl)sulfonyl]amino]acetyl]amino]-3-(4-morpholinyl)-3 -oxopropyl]-, methyl ester, monohydrochloride

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Technology Process of Benzenecarboximidic acid, 4-[2-[[[[(4-methylphenyl)sulfonyl]amino]acetyl]amino]-3-(4-morpholinyl)-3 -oxopropyl]-, methyl ester, monohydrochloride

There total 6 articles about Benzenecarboximidic acid, 4-[2-[[[[(4-methylphenyl)sulfonyl]amino]acetyl]amino]-3-(4-morpholinyl)-3 -oxopropyl]-, methyl ester, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 84792-54-1
N-[1-(4-Cyano-benzyl)-2-morpholin-4-yl-2-oxo-ethyl]-2-(toluene-4-sulfonylamino)-acetamide

: 84792-55-2
4-{3-Morpholin-4-yl-3-oxo-2-[2-(toluene-4-sulfonylamino)-acetylamino]-propyl}-benzimidic acid methyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; at 5 ℃; for 48h;

Reference yield:

: 52117-01-8
N-acetyl-4-cyano-α-(ethoxycarbonyl)phenylalanine ethyl ester

: 84792-55-2
4-{3-Morpholin-4-yl-3-oxo-2-[2-(toluene-4-sulfonylamino)-acetylamino]-propyl}-benzimidic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: NaOH (1 mol/l) / acetic acid; H₂O / pH 3.8-4.0

2: NaOH (1 mol/l) / diethyl ether; ethyl acetate; H₂O / 10 h

3: 60 percent / DCC / pyridine / 12 h / Ambient temperature

4: 40 percent / pyridine; dimethylformamide / 7 h / Ambient temperature

5: 80 percent / HCl-gas in abs.MeOH (1,0 g/2ml) / dioxane; methanol / 48 h / 5 °C

With hydrogenchloride; sodium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; methanol; diethyl ether; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 56218-62-3
2-(4-methylphenylsulfonamido)acetyl chloride

: 84792-55-2
4-{3-Morpholin-4-yl-3-oxo-2-[2-(toluene-4-sulfonylamino)-acetylamino]-propyl}-benzimidic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH (1 mol/l) / diethyl ether; ethyl acetate; H₂O / 10 h

2: 60 percent / DCC / pyridine / 12 h / Ambient temperature

3: 40 percent / pyridine; dimethylformamide / 7 h / Ambient temperature

4: 80 percent / HCl-gas in abs.MeOH (1,0 g/2ml) / dioxane; methanol / 48 h / 5 °C

With hydrogenchloride; sodium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; methanol; diethyl ether; water; ethyl acetate; N,N-dimethyl-formamide;