L-Leucine, N-[(1,1-dimethylethoxy)carbonyl]-, 2-[4-[[(2-aminoethyl)amino]carbonyl]phenyl]hydrazide

Base Information

Chemical Name:L-Leucine, N-[(1,1-dimethylethoxy)carbonyl]-, 2-[4-[[(2-aminoethyl)amino]carbonyl]phenyl]hydrazide
CAS No.:848083-55-6
Molecular Formula:C20H33N5O4
Molecular Weight:407.513
Hs Code.:

Synonyms:

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Chemical Property of L-Leucine, N-[(1,1-dimethylethoxy)carbonyl]-, 2-[4-[[(2-aminoethyl)amino]carbonyl]phenyl]hydrazide

Chemical Property:

Purity/Quality:

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Technology Process of L-Leucine, N-[(1,1-dimethylethoxy)carbonyl]-, 2-[4-[[(2-aminoethyl)amino]carbonyl]phenyl]hydrazide

There total 4 articles about L-Leucine, N-[(1,1-dimethylethoxy)carbonyl]-, 2-[4-[[(2-aminoethyl)amino]carbonyl]phenyl]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848083-53-4
C₂₈H₃₉N₅O₆

: 848083-55-6
(2S)-N-({4-[N-(2-aminoethyl)carbamoyl]phenyl}amino)-2-[(tert-butoxy)carbonylamino]-4-methylpentanamide

Guidance literature:: With hydrogen; palladium on carbon; In ethanol; for 20h; under 3102.97 Torr;

Reference yield:

: C₁₇H₂₀N₄O₃

: 848083-55-6
(2S)-N-({4-[N-(2-aminoethyl)carbamoyl]phenyl}amino)-2-[(tert-butoxy)carbonylamino]-4-methylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

2: hydrogen / palladium on carbon / ethanol / 20 h / 3102.97 Torr

With hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on carbon; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 96736-00-4
4-(2-(tert-butoxycarbonyl)hydrazineyl)benzoic acid

: 848083-55-6
(2S)-N-({4-[N-(2-aminoethyl)carbamoyl]phenyl}amino)-2-[(tert-butoxy)carbonylamino]-4-methylpentanamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 16 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

4: hydrogen / palladium on carbon / ethanol / 20 h / 3102.97 Torr

With hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; trifluoroacetic acid; palladium on carbon; In ethanol; dichloromethane; N,N-dimethyl-formamide;