(4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide

Base Information

Chemical Name:(4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide
CAS No.:848083-52-3
Molecular Formula:C₂₂H₂₈N₄O₅
Molecular Weight:428.488
Hs Code.:

Synonyms:(4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide

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Chemical Property of (4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide

Chemical Property:

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Technology Process of (4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide

There total 1 articles about (4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.8%

: 96736-00-4
4-(2-(tert-butoxycarbonyl)hydrazineyl)benzoic acid

: 18807-71-1
benzyl N-(2-aminoethyl)carbamate hydrochloride

: 848083-52-3
(4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 848083-52-3
(4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide

: C₁₇H₂₀N₄O₃

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.166667h;

Reference yield:

: 848083-52-3
(4-{[(tert-butoxy)carbonylamino]amino}phenyl)-N-{2-[(phenylmethoxy)carbonylamino]ethyl}carboxamide

: 848083-55-6
(2S)-N-({4-[N-(2-aminoethyl)carbamoyl]phenyl}amino)-2-[(tert-butoxy)carbonylamino]-4-methylpentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C

3: hydrogen / palladium on carbon / ethanol / 20 h / 3102.97 Torr

With hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on carbon; In ethanol; dichloromethane; N,N-dimethyl-formamide;