2-cyano-N-(pyridin-2-ylmethyl)acetamide

Base Information

• Chemical Name: 2-cyano-N-(pyridin-2-ylmethyl)acetamide
• CAS No.: 84951-58-6
• Molecular Formula: C9H9N3O
• Molecular Weight: 175.19
• Hs Code.: 2933399090
• Mol file: 84951-58-6.mol

Synonyms:Cyan-essigsaeure-phenaethylamid;N-(cyanoacetyl)phenylethylamide;2-cyano-N-(2-pyridylmethyl)acetamide;cyano-acetic acid phenethylamide;2-cyano-n-phenethyl-acetamide;2-cyano-N-(2-phenylethyl)ethanamide;

Chemical Property of 2-cyano-N-(pyridin-2-ylmethyl)acetamide

Chemical Property:

• PSA: 65.78000
• LogP: 1.00238

Purity/Quality:

2-Cyano-N-(pyridin-2-ylmethyl)acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-cyano-N-(pyridin-2-ylmethyl)acetamide

There total 4 articles about 2-cyano-N-(pyridin-2-ylmethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(Aminomethyl)pyridine (3731-51-9) + methyl 2-cyanoacetate (105-34-0) → 2-cyano-N-(pyridin-2-ylmethyl)acetamide (84951-58-6)

Guidance literature:

at 0 - 20 ℃; Neat (no solvent);

DOI:10.1016/j.bmc.2011.10.061

Reference yield: 93.8%

2-aminopyridine (504-29-0) + methyl 2-cyanoacetate (105-34-0) → 2-cyano-N-(pyridin-2-ylmethyl)acetamide (84951-58-6)

Guidance literature:

In neat (no solvent); at 20 ℃; for 4h;

DOI:10.1071/CH16648

Reference yield:

2-(Aminomethyl)pyridine (3731-51-9) + cyanoacetic acid (372-09-8) → 2-cyano-N-(pyridin-2-ylmethyl)acetamide (84951-58-6)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate;

DOI:10.1016/j.bmcl.2013.01.014

upstream raw materials:

2-(Aminomethyl)pyridine

methyl 2-cyanoacetate

cyanoacetic acid

2-aminopyridine

Downstream raw materials:

(E)-2-cyano-3-(4-hydroxyphenyl)-N-(pyridin-2-ylmethyl)acrylamide

(E)-2-cyano-3-[4-(dimethylamino)phenyl]-N-(pyridin-2-ylmethyl)acrylamide

(E)-2-cyano-3-(4-isopropylphenyl)-N-(pyridin-2-ylmethyl)acrylamide

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