Technology Process of Diazene, phenyl[2,3,5-trichloro-4-(hexyloxy)-6-(propylthio)phenyl]-
There total 5 articles about Diazene, phenyl[2,3,5-trichloro-4-(hexyloxy)-6-(propylthio)phenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide; cetyltributylphosphonium bromide;
In
toluene;
for 3h;
DOI:10.1016/j.tet.2005.01.023
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 91 percent / anhydrous K2CO3; Aliquat(R)336 / acetonitrile / Heating
2: 78 percent / KOH; hexadecyltributylphosphonium bromide / toluene / 3 h
With
potassium hydroxide; Aliquat 336; cetyltributylphosphonium bromide; potassium carbonate;
In
toluene; acetonitrile;
DOI:10.1016/j.tet.2005.01.023
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 80 percent / BBr3 / CH2Cl2 / 0 - 20 °C
2.1: HCl; NaNO2 / H2O
2.2: 44 percent / urea; NaOH / H2O / 0 - 20 °C
3.1: 91 percent / anhydrous K2CO3; Aliquat(R)336 / acetonitrile / Heating
4.1: 78 percent / KOH; hexadecyltributylphosphonium bromide / toluene / 3 h
With
hydrogenchloride; potassium hydroxide; boron tribromide; Aliquat 336; cetyltributylphosphonium bromide; potassium carbonate; sodium nitrite;
In
dichloromethane; water; toluene; acetonitrile;
DOI:10.1016/j.tet.2005.01.023
