2,3,5,6-Tetrachloroanisole

Base Information

Chemical Name:2,3,5,6-Tetrachloroanisole
CAS No.:6936-40-9
Molecular Formula:C7H4 Cl4 O
Molecular Weight:245.92
Hs Code.:2909309090
European Community (EC) Number:230-061-0
NSC Number:21468
UNII:64764RMB8N
DSSTox Substance ID:DTXSID30863963
Nikkaji Number:J131.499H
Wikidata:Q27263711
Mol file:6936-40-9.mol

Synonyms:2,3,5,6-Tetrachloroanisole;6936-40-9;1,2,4,5-TETRACHLORO-3-METHOXYBENZENE;Anisole, 2,3,5,6-tetrachloro-;Benzene, 1,2,4,5-tetrachloro-3-methoxy-;Tetrachloromethoxybenzene;EINECS 230-061-0;NSC 21468;Benzene, tetrachloromethoxy-;Benzene,1,2,4,5-tetrachloro-3-methoxy-;UNII-64764RMB8N;AI3-22330;64764RMB8N;NSC-21468;53452-81-6;1,2,4,5-Tetrachloro-3-methoxy-benzene;Anisole,3,5,6-tetrachloro-;SCHEMBL8640622;DTXSID30863963;NSC21468;AKOS024319708;Benzene,2,4,5-tetrachloro-3-methoxy-;LS-20222;1,2,4,5-Tetrachloro-3-methoxybenzene #;FT-0636292;2,3,5,6-Tetrachloroanisole, analytical standard;Q27263711;2,3,5,6-Tetrachloroanisole 10 microg/mL in Isooctane

Suppliers and Price of 2,3,5,6-Tetrachloroanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2,3,5,6-Tetrachloroanisole analytical standard
100mg
$ 110.00

American Custom Chemicals Corporation
2,3,5,6-TETRACHLOROANISOLE 95.00%
5MG
$ 496.27

Total 12 raw suppliers

Chemical Property of 2,3,5,6-Tetrachloroanisole

Chemical Property:

Vapor Pressure:0.00442mmHg at 25°C
Boiling Point:286.9°C at 760 mmHg
Flash Point:113.6°C
PSA：9.23000
Density:1.525g/cm³
LogP:4.30880
Storage Temp.:2-8°C
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:245.898675
Heavy Atom Count:12
Complexity:140

Purity/Quality:

99% ^*data from raw suppliers

2,3,5,6-Tetrachloroanisole analytical standard ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22-37/38-53
Safety Statements: 37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=CC(=C1Cl)Cl)Cl)Cl

Technology Process of 2,3,5,6-Tetrachloroanisole

There total 14 articles about 2,3,5,6-Tetrachloroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 67-56-1
methanol

: 117-18-0
2,3,5,6-Tetrachloronitrobenzene

: 6936-40-9
2,3,5,6-tetrachloroanisole

Guidance literature:: With sodium methylate; In tetrahydrofuran; at 60 ℃; for 4h;
DOI:10.1016/j.tet.2005.01.023

Reference yield:

: 117-18-0
2,3,5,6-Tetrachloronitrobenzene

: 6936-40-9
2,3,5,6-tetrachloroanisole

Guidance literature:: With /BRN= 3592982/; In methanol; at 37.9 - 60.4 ℃; Kinetics;
DOI:10.1039/P29760001541

Reference yield:

: 3481-20-7
2,3,5,6-tetrachloroaniline

: 6936-40-9
2,3,5,6-tetrachloroanisole

Guidance literature:: Multi-step reaction with 3 steps

1: concentrated sulfuric acid / Diazotization_.Behandeln mit salzsaurer Kupfer(I)-chlorid-Loesung

2: sodium methylate solution / 180 °C / im Rohr

3: alkali

With sulfuric acid; sodium methylate;