Carbamic acid, [(1S)-1-[[[(1S)-2-amino-2-oxo-1-(phenylmethyl)ethyl]amino]carbonyl]-3-[[ (1,1-dimethylethoxy)carbonyl]amino]propyl]-, 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-1-[[[(1S)-2-amino-2-oxo-1-(phenylmethyl)ethyl]amino]carbonyl]-3-[[ (1,1-dimethylethoxy)carbonyl]amino]propyl]-, 9H-fluoren-9-ylmethyl ester
CAS No.:849948-77-2
Molecular Formula:C33H38N4O6
Molecular Weight:586.688
Hs Code.:

Carbamic acid,
[(1S)-1-[[[(1S)-2-amino-2-oxo-1-(phenylmethyl)ethyl]amino]carbonyl]-3-[[
(1,1-dimethylethoxy)carbonyl]amino]propyl]-, 9H-fluoren-9-ylmethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [(1S)-1-[[[(1S)-2-amino-2-oxo-1-(phenylmethyl)ethyl]amino]carbonyl]-3-[[ (1,1-dimethylethoxy)carbonyl]amino]propyl]-, 9H-fluoren-9-ylmethyl ester

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Technology Process of Carbamic acid, [(1S)-1-[[[(1S)-2-amino-2-oxo-1-(phenylmethyl)ethyl]amino]carbonyl]-3-[[ (1,1-dimethylethoxy)carbonyl]amino]propyl]-, 9H-fluoren-9-ylmethyl ester

There total 1 articles about Carbamic acid, [(1S)-1-[[[(1S)-2-amino-2-oxo-1-(phenylmethyl)ethyl]amino]carbonyl]-3-[[ (1,1-dimethylethoxy)carbonyl]amino]propyl]-, 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 65864-22-4
(S)-2-amino-3-phenylpropionamide hydrochloride

: 125238-99-5,114360-56-4
(S)-4-tert-butoxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)butyric acid

: 849948-77-2
(1'S, 2S)-4-(N-Boc-amino)-N'-(1'-carbamoyl-2'-phenylethyl)-2-(N''-Fmoc-amino)butanamide

Guidance literature:: With benzotriazol-1-ol; triethylamine; diisopropyl-carbodiimide; In DMF (N,N-dimethyl-formamide); dichloromethane;

Reference yield:

: 849948-77-2
(1'S, 2S)-4-(N-Boc-amino)-N'-(1'-carbamoyl-2'-phenylethyl)-2-(N''-Fmoc-amino)butanamide

: 17337-81-4
(S)-2-amino-4-(N-Boc-amino)-N'-((S)-1-carbamoyl-2-phenylethyl)butanamide

Guidance literature:: With piperidine; In DMF (N,N-dimethyl-formamide); for 0.75h;

Reference yield:

: 849948-77-2
(1'S, 2S)-4-(N-Boc-amino)-N'-(1'-carbamoyl-2'-phenylethyl)-2-(N''-Fmoc-amino)butanamide

: 10447-11-7
4-methyl-1-naphthalenesulfonyl chloride

: J-2156

Guidance literature:: (1'S, 2S)-4-(N-Boc-amino)-N'-(1'-carbamoyl-2'-phenylethyl)-2-(N''-Fmoc-amino)butanamide; With piperidine; In N,N-dimethyl-formamide; for 0.75h;

4-methyl-1-naphthalenesulfonyl chloride; In tetrahydrofuran; N,N-dimethyl-formamide; for 16h;

With trifluoroacetic acid; In dichloromethane; for 1h;
DOI:10.1124/jpet.104.075531