Benzene, 2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)-

Base Information

Chemical Name:Benzene, 2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)-
CAS No.:851182-68-8
Molecular Formula:C10H13BrO3
Molecular Weight:261.115
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)-

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Technology Process of Benzene, 2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)-

There total 3 articles about Benzene, 2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25458-46-2
4-methoxyphenyl methoxymethyl ether

: 851182-68-8
2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-butyllithium / diethyl ether / 3 h / 20 °C

1.2: 80 percent / diethyl ether / 0.5 h

2.1: 95 percent / sodium borohydride / methanol / 3 h / 20 °C

3.1: 90 percent / N-bromosuccinimide; dimethyl sulfide / CH₂Cl₂ / 4 h / 0 °C

With sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; dimethylsulfide; In methanol; diethyl ether; dichloromethane; 3.1: Corey reaction;
DOI:10.1016/j.bmc.2005.02.010

Reference yield:

: 73220-20-9
5-methoxy-2-(methoxymethoxy)benzaldehyde

: 851182-68-8
2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / sodium borohydride / methanol / 3 h / 20 °C

2: 90 percent / N-bromosuccinimide; dimethyl sulfide / CH₂Cl₂ / 4 h / 0 °C

With sodium tetrahydroborate; N-Bromosuccinimide; dimethylsulfide; In methanol; dichloromethane; 2: Corey reaction;
DOI:10.1016/j.bmc.2005.02.010

Reference yield:

: 150-76-5
4-methoxy-phenol

: 851182-68-8
2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / diethyl ether

2.1: N-butyllithium / diethyl ether / 3 h / 20 °C

2.2: 80 percent / diethyl ether / 0.5 h

3.1: 95 percent / sodium borohydride / methanol / 3 h / 20 °C

4.1: 90 percent / N-bromosuccinimide; dimethyl sulfide / CH₂Cl₂ / 4 h / 0 °C

With sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; dimethylsulfide; sodium hydride; In methanol; diethyl ether; dichloromethane; 4.1: Corey reaction;
DOI:10.1016/j.bmc.2005.02.010