2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene

Base Information

Chemical Name:2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene
CAS No.:851182-77-9
Molecular Formula:C₂₄H₃₄O₃
Molecular Weight:370.532
Hs Code.:

Synonyms:2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene

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Chemical Property of 2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene

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Technology Process of 2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene

There total 11 articles about 2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 851182-75-7
2-((5-methoxy-2-(methoxymethoxy)phenyl)methyl)-1,3-methylcyclohex-3-enecarbaldehyde

: 51795-72-3
diethyl 3-methylbut-2-enylphosphonate

: 851182-77-9
2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene

Guidance literature:: diethyl 3-methylbut-2-enylphosphonate; With lithium diisopropyl amide; In tetrahydrofuran; for 0.5h;

2-((5-methoxy-2-(methoxymethoxy)phenyl)methyl)-1,3-methylcyclohex-3-enecarbaldehyde; In tetrahydrofuran; for 4h;
DOI:10.1016/j.bmc.2005.02.010

Reference yield:

: 851182-68-8
2-(bromomethyl)-4-methoxy-1-(methoxymethoxy)benzene

: 851182-77-9
2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: 70 percent / LiHMDS; HMPA / tetrahydrofuran / 0.42 h / -92 °C

2.1: 86 percent / pyridine / 3 h / Heating

3.1: 78 percent / hydroquinone / toluene / 2 h / 90 °C

4.1: 55 percent / NaH / tetrahydrofuran / 4 h / 20 °C

5.1: LDA / tetrahydrofuran / 0.5 h

5.2: 19 percent / tetrahydrofuran / 4 h

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride; hydroquinone; lithium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; toluene; 3.1: Diels-Alder reaction / 5.1: Horner-Emmons reaction;
DOI:10.1016/j.bmc.2005.02.010

Reference yield:

: 4-methoxy-1-(methoxymethoxy)-2-(3-methylpenta-2,4-dienyl)benzene

: 851182-77-9
2-((2,6-dimethyl-6-(4-methylpenta-1,3-dienyl)cyclohex-2-enyl)methyl)-4-methoxy-1-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 78 percent / hydroquinone / toluene / 2 h / 90 °C

2.1: 55 percent / NaH / tetrahydrofuran / 4 h / 20 °C

3.1: LDA / tetrahydrofuran / 0.5 h

3.2: 19 percent / tetrahydrofuran / 4 h

With sodium hydride; hydroquinone; lithium diisopropyl amide; In tetrahydrofuran; toluene; 1.1: Diels-Alder reaction / 3.1: Horner-Emmons reaction;
DOI:10.1016/j.bmc.2005.02.010