Technology Process of Cyclohexanecarboxylic acid,
4-acetyl-2-[(1,4-dimethoxy-2-naphthalenyl)carbonyl]-, methyl ester
There total 10 articles about Cyclohexanecarboxylic acid,
4-acetyl-2-[(1,4-dimethoxy-2-naphthalenyl)carbonyl]-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
for 2h;
under 1034.3 Torr;
DOI:10.1021/jo00157a039
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 85 percent / AlCl3 / various solvent(s) / Ambient temperature
2: 1.) Br2, 2.) Et3N / 1.) CCl4, room temp., 4 h, 2.) CCl4, room temp.
3: 70 percent / toluene / 60 h / Heating
4: 65 percent / N-chlorosuccinimide, AgNO3 / acetonitrile; H2O / 0.5 h
5: H2 / 10percent Pd/C / ethanol / 2 h / 1034.3 Torr
With
N-chloro-succinimide; aluminium trichloride; hydrogen; bromine; silver nitrate; triethylamine;
palladium on activated charcoal;
In
ethanol; water; toluene; acetonitrile;
DOI:10.1021/jo00157a039
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / toluene / 60 h / Heating
2: 65 percent / N-chlorosuccinimide, AgNO3 / acetonitrile; H2O / 0.5 h
3: H2 / 10percent Pd/C / ethanol / 2 h / 1034.3 Torr
With
N-chloro-succinimide; hydrogen; silver nitrate;
palladium on activated charcoal;
In
ethanol; water; toluene; acetonitrile;
DOI:10.1021/jo00157a039