4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid

Base Information

Chemical Name:4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid
CAS No.:85293-77-2
Molecular Formula:C₂₂H₂₄O₆
Molecular Weight:384.429
Hs Code.:

Synonyms:4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid

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Chemical Property of 4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid

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Technology Process of 4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid

There total 8 articles about 4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85293-76-1
4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid methyl ester

: 85293-77-2
4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid

Guidance literature:: With sodium hydroxide; In methanol; at 60 ℃; for 12h;
DOI:10.1021/jo00157a039

Reference yield:

: 10075-62-4
1,4-dimethoxynaphthalene

: 85293-77-2
4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / AlCl₃ / various solvent(s) / Ambient temperature

2: 1.) Br₂, 2.) Et₃N / 1.) CCl₄, room temp., 4 h, 2.) CCl₄, room temp.

3: 70 percent / toluene / 60 h / Heating

4: 65 percent / N-chlorosuccinimide, AgNO₃ / acetonitrile; H₂O / 0.5 h

5: H₂ / 10percent Pd/C / ethanol / 2 h / 1034.3 Torr

6: 2N NaOH / methanol / 12 h / 60 °C

With sodium hydroxide; N-chloro-succinimide; aluminium trichloride; hydrogen; bromine; silver nitrate; triethylamine; palladium on activated charcoal; In methanol; ethanol; water; toluene; acetonitrile;
DOI:10.1021/jo00157a039

Reference yield:

: 85293-68-1
2-Methyl-2-(1-methylene-allyl)-[1,3]dithiolane

: 85293-77-2
4-Acetyl-2-(1,4-dimethoxy-naphthalene-2-carbonyl)-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / toluene / 60 h / Heating

2: 65 percent / N-chlorosuccinimide, AgNO₃ / acetonitrile; H₂O / 0.5 h

3: H₂ / 10percent Pd/C / ethanol / 2 h / 1034.3 Torr

4: 2N NaOH / methanol / 12 h / 60 °C

With sodium hydroxide; N-chloro-succinimide; hydrogen; silver nitrate; palladium on activated charcoal; In methanol; ethanol; water; toluene; acetonitrile;
DOI:10.1021/jo00157a039