Cyclohept[b]indole, 5,5a,6,7,8,9,10,10a-octahydro-

Base Information

Chemical Name:Cyclohept[b]indole, 5,5a,6,7,8,9,10,10a-octahydro-
CAS No.:855405-55-9
Molecular Formula:C₁₃H₁₇N
Molecular Weight:187.285
Hs Code.:
Mol file:855405-55-9.mol

Synonyms:Cyclohept[b]indole;CYCLOHEPT[B]INDOLE, 5,5A,6,7,8,9,10,10A-OCTAHYDRO-;5,5A,6,7,8,9,10,10A-OCTAHYDRO-CYCLOHEPT[B]INDOLE;

Suppliers and Price of Cyclohept[b]indole, 5,5a,6,7,8,9,10,10a-octahydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Cyclohept[b]indole, 5,5a,6,7,8,9,10,10a-octahydro-

Chemical Property:

PSA：12.03000
LogP:3.66640

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohept[b]indole, 5,5a,6,7,8,9,10,10a-octahydro-

There total 11 articles about Cyclohept[b]indole, 5,5a,6,7,8,9,10,10a-octahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2047-89-4
5,6,7,8,9,10-hexahydrocyclohept[b]indole

: 855405-55-9
5,5a,6,7,8,9,10,10a-octahydrocyclohept[b]indole

Guidance literature:: With palladium(II) trifluoroacetate; 2,2,2-trifluoroethanol; (R)-10-camphorsulfonic acid; hydrogen; (R)-(+)-2,2'-bis(diphenylphosphanyl)-5,5',6,6',7,7',8,8'-octahydro-1,1'-binaphthyl; In dichloromethane; at 20 ℃; for 24h; under 36201.3 Torr; optical yield given as %ee; enantioselective reaction; Autoclave;
DOI:10.1021/ja103668q

Reference yield:

: 2047-89-4
5,6,7,8,9,10-hexahydrocyclohept[b]indole

: 855405-55-9
5,5a,6,7,8,9,10,10a-octahydrocyclohepta[b]indole

Guidance literature:: With palladium(II) trifluoroacetate; 5,5'-decamethylenedioxy-2,2'-bis(diphenylphosphino)biphenyl; (1S)-10-camphorsulfonic acid; hydrogen; In dichloromethane; at 35 ℃; for 24h; under 45004.5 Torr; enantioselective reaction; Autoclave;
DOI:10.1016/j.tet.2013.06.016