Butanedioic acid, 2,3-bis[(4-methylbenzoyl)oxy]-, (2R,3R)-, compd. with ethyl 3-(2-amino-2-methylpropyl)benzeneacetate (1:1)

Base Information Edit

Chemical Name:Butanedioic acid, 2,3-bis[(4-methylbenzoyl)oxy]-, (2R,3R)-, compd. with ethyl 3-(2-amino-2-methylpropyl)benzeneacetate (1:1)
CAS No.:861448-90-0
Molecular Formula:C20H18O8.C14H21NO2
Molecular Weight:621.684
Hs Code.:
Mol file:861448-90-0.mol

Synonyms:

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Chemical Property of Butanedioic acid, 2,3-bis[(4-methylbenzoyl)oxy]-, (2R,3R)-, compd. with ethyl 3-(2-amino-2-methylpropyl)benzeneacetate (1:1) Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanedioic acid, 2,3-bis[(4-methylbenzoyl)oxy]-, (2R,3R)-, compd. with ethyl 3-(2-amino-2-methylpropyl)benzeneacetate (1:1)

There total 5 articles about Butanedioic acid, 2,3-bis[(4-methylbenzoyl)oxy]-, (2R,3R)-, compd. with ethyl 3-(2-amino-2-methylpropyl)benzeneacetate (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 808768-94-7
ethyl 2-[3-(2-amino-2-methylpropyl)phenyl]acetate

: 32634-66-5
Di-p-toluoyl-L-tartaric acid

: 861448-90-0
ethyl 2-[3-(2-amino-2-methylpropyl)phenyl]acetate hydrogen (2R,3R)-2,3-bis[(4-methylbenzoyl)oxy]succinate

Guidance literature:: In acetonitrile; for 3h;

Reference yield:

: 808768-96-9
2-[3-(2-hydroxy-2-methylpropyl)phenyl]acetic acid

: 861448-90-0
ethyl 2-[3-(2-amino-2-methylpropyl)phenyl]acetate hydrogen (2R,3R)-2,3-bis[(4-methylbenzoyl)oxy]succinate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; acetic acid / dichloromethane / 5 - 20 °C / Large scale reaction

2: sulfuric acid / 1.5 h / Reflux; Large scale reaction

3: acetic acid; thiourea / ethanol / 4 h / Reflux

4: acetonitrile / 15 h / 20 °C / Large scale reaction

With sulfuric acid; acetic acid; thiourea; In ethanol; dichloromethane; acetonitrile; 1: Ritter reaction;
DOI:10.1021/op200108k

Reference yield:

: 808768-95-8
(3-{2-[(chloroacetyl)amino]-2-methylpropyl}phenyl)acetic acid

: 861448-90-0
ethyl 2-[3-(2-amino-2-methylpropyl)phenyl]acetate hydrogen (2R,3R)-2,3-bis[(4-methylbenzoyl)oxy]succinate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 1.5 h / Reflux; Large scale reaction

2: acetic acid; thiourea / ethanol / 4 h / Reflux

3: acetonitrile / 15 h / 20 °C / Large scale reaction

With sulfuric acid; acetic acid; thiourea; In ethanol; acetonitrile;
DOI:10.1021/op200108k