5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid benzylidenehydrazide

Base Information

Chemical Name:5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid benzylidenehydrazide
CAS No.:94772-02-8
Molecular Formula:C₁₈H₁₈N₆O₃
Molecular Weight:366.379
Hs Code.:

Synonyms:BRN 4573488;5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid benzylidenehydrazide;94772-02-8;5-(3,4-Dimethoxyphenyl)-2H-tetrazole-2-acetic acid (phenylmethylene)hydrazide;2H-Tetrazole-2-acetic acid, 5-(3,4-dimethoxyphenyl)-, (phenylmethylene)hydrazide

Suppliers and Price of 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid benzylidenehydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-(3,4-DIMETHOXYPHENYL)-2H-TETRAZOLE-2-ACETIC ACID (PHENYLMETHYLENE)HYDRAZIDE 95.00%
5MG
$ 499.82

Total 0 raw suppliers

Chemical Property of 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid benzylidenehydrazide

Chemical Property:

Melting Point:200 °C(Solv: ethanol (64-17-5))
PSA：107.01000
Density:1.31±0.1 g/cm3(Predicted)
LogP:2.34790
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:366.14403846
Heavy Atom Count:27
Complexity:500

Purity/Quality:: 5-(3,4-DIMETHOXYPHENYL)-2H-TETRAZOLE-2-ACETIC ACID (PHENYLMETHYLENE)HYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C2=NN(N=N2)CC(=O)NN=CC3=CC=CC=C3)OC
Isomeric SMILES:COC1=C(C=C(C=C1)C2=NN(N=N2)CC(=O)N/N=C/C3=CC=CC=C3)OC

Technology Process of 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid benzylidenehydrazide

There total 4 articles about 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid benzylidenehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 94771-93-4
5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid hydrazide

: 100-52-7
benzaldehyde

: 94772-02-8
[5-(3,4-Dimethoxy-phenyl)-tetrazol-2-yl]-acetic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: With acetic acid; In ethanol; Heating;

Reference yield:

: 2024-83-1
veratronitrile

: 94772-02-8
[5-(3,4-Dimethoxy-phenyl)-tetrazol-2-yl]-acetic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / NaN₃, NH₄Cl / dimethylformamide / 127 °C

2: 70 percent / NaOEt / ethanol / 16 h / Heating

3: 65 percent / 99percent H₂H₄*H₂O / ethanol / 8 h / Heating

4: 55 percent / AcOH / ethanol / Heating

With sodium azide; sodium ethanolate; ammonium chloride; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 10493-27-3
5-(3,4-Dimethoxyphenyl)tetrazole

: 94772-02-8
[5-(3,4-Dimethoxy-phenyl)-tetrazol-2-yl]-acetic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / NaOEt / ethanol / 16 h / Heating

2: 65 percent / 99percent H₂H₄*H₂O / ethanol / 8 h / Heating

3: 55 percent / AcOH / ethanol / Heating

With sodium ethanolate; hydrazine hydrate; acetic acid; In ethanol;