1-(3,7-dinitro-5-oxido-10H-phenothiazin-10-yl)ethanone

Base Information

• Chemical Name: 1-(3,7-dinitro-5-oxido-10H-phenothiazin-10-yl)ethanone
• CAS No.: 7506-02-7
• Molecular Formula: C₁₄H₉N₃O₆S
• Molecular Weight: 347.308
• Mol file: 7506-02-7.mol

Synonyms:10H-Phenothiazine,10-acetyl-3,7-dinitro-, 5-oxide (9CI); Phenothiazine, 10-acetyl-3,7-dinitro-,5-oxide (8CI); NSC 402441

Chemical Property of 1-(3,7-dinitro-5-oxido-10H-phenothiazin-10-yl)ethanone

Chemical Property:

• Vapor Pressure: 7.92E-22mmHg at 25°C
• Boiling Point: 741°Cat760mmHg
• Flash Point: 402°C
• Density: 1.73g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3,7-dinitro-5-oxido-10H-phenothiazin-10-yl)ethanone

There total 3 articles about 1-(3,7-dinitro-5-oxido-10H-phenothiazin-10-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10H-phenothiazine (92-84-2) → 10-acetyl-3,7-dinitro-10H-phenothiazine 5-oxide (7506-02-7)

Guidance literature:

With nitric acid; acetic acid;

DOI:10.1021/ja01234a013

Reference yield:

1-(3,7-dinitrophenothiazin-10-yl)-ethanone (1628-79-1) → 10-acetyl-3,7-dinitro-10H-phenothiazine 5-oxide (7506-02-7)

Guidance literature:

With nitric acid; In 1,4-dioxane;

DOI:10.1007/BF00475284

Reference yield:

3,11-dinitro-10H-phenothiazine (1747-90-6) → 10-acetyl-3,7-dinitro-10H-phenothiazine 5-oxide (7506-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Py / Heating

2: aq. HNO₃ / dioxane

With pyridine; nitric acid; In 1,4-dioxane;

DOI:10.1007/BF00475284

upstream raw materials:

10H-phenothiazine

1-(3,7-dinitrophenothiazin-10-yl)-ethanone

3,11-dinitro-10H-phenothiazine