1-Pyrrolidinecarboxaldehyde, 2-[3-(4-methoxyphenyl)-2-oxopropyl]-

Base Information

Chemical Name:1-Pyrrolidinecarboxaldehyde, 2-[3-(4-methoxyphenyl)-2-oxopropyl]-
CAS No.:87264-39-9
Molecular Formula:C15H19NO3
Molecular Weight:261.31600
Hs Code.:

Synonyms:1-(1-formylpyrrolidin-2-yl)-3-(4-methoxyphenyl)propan-2-one;1-Pyrrolidinecarboxaldehyde,2-[3-(4-methoxyphenyl)-2-oxopropyl];

Suppliers and Price of 1-Pyrrolidinecarboxaldehyde, 2-[3-(4-methoxyphenyl)-2-oxopropyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Pyrrolidinecarboxaldehyde, 2-[3-(4-methoxyphenyl)-2-oxopropyl]-

Chemical Property:

PSA：46.61000
LogP:2.39150

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Pyrrolidinecarboxaldehyde, 2-[3-(4-methoxyphenyl)-2-oxopropyl]-

There total 4 articles about 1-Pyrrolidinecarboxaldehyde, 2-[3-(4-methoxyphenyl)-2-oxopropyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 87264-38-8
1-formyl-2β-<(2R*)-hydroxy-3-(4-methoxyphenyl)propyl>pyrrolidine

: 87264-39-9
1-(1-formylpyrrolidin-2-yl)-3-(4-methoxyphenyl)propan-2-one

Guidance literature:: With Collins oxidation agent; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 140-67-0
Estragole

: 87264-39-9
1-(1-formylpyrrolidin-2-yl)-3-(4-methoxyphenyl)propan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / toluene / Heating

2: 82 percent / H₂ / 10 percent Pd/C

3: 2.) ammonia / 1.) toluene, heating; 2.) methanol

4: 72 percent / CH₂Cl₂ / Ambient temperature; Collins oxidation

With ammonia; hydrogen; palladium on activated charcoal; In dichloromethane; toluene;
DOI:10.1246/cl.1983.1195

Reference yield:

: 87264-35-5
trans-2,3,3a,4,5,6-hexahydro-2-(4-methoxybenzyl)pyrrolo-<1,2-b>isoxazole

: 87264-39-9
1-(1-formylpyrrolidin-2-yl)-3-(4-methoxyphenyl)propan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / H₂ / 10 percent Pd/C

2: 2.) ammonia / 1.) toluene, heating; 2.) methanol

3: 72 percent / CH₂Cl₂ / Ambient temperature; Collins oxidation

With ammonia; hydrogen; palladium on activated charcoal; In dichloromethane;
DOI:10.1246/cl.1983.1195