(S)-2-N-Boc-aminomethylmorpholine

Base Information

• Chemical Name: (S)-2-N-Boc-aminomethylmorpholine
• CAS No.: 875551-59-0
• Molecular Formula: C10H20N2O3
• Molecular Weight: 216.28
• Hs Code.: 2934999090
• Mol file: 875551-59-0.mol

Synonyms:tert-butyl N-[[(2S)-morpholin-2-yl]methyl]carbamate;

Chemical Property of (S)-2-N-Boc-aminomethylmorpholine

Chemical Property:

• Vapor Pressure: 0.000131mmHg at 25°C
• Boiling Point: 334.0±17.0 °C(Predicted)
• PKA: 12.22±0.46(Predicted)
• PSA: 59.59000
• Density: 1.032±0.06 g/cm3(Predicted)
• LogP: 1.21920
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

(S)-2-(N-Boc-aminomethyl)morpholine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-2-N-Boc-aminomethylmorpholine

There total 3 articles about (S)-2-N-Boc-aminomethylmorpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dimethylethyl {[(2R)-4-(phenylmethyl)-2-morpholinyl]methyl}carbamate (875551-47-6) → tert-butyl N-[[(2S)-morpholin-2-yl]methyl]carbamate (875551-59-0)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; for 43h; under 760.051 Torr;

Reference yield:

1,1-dimethylethyl ({(2S)-4-[(3,4-dichlorophenyl)methyl]-2-morpholinyl}methyl)carbamate (956010-37-0) → tert-butyl N-[[(2S)-morpholin-2-yl]methyl]carbamate (875551-59-0)

Guidance literature:

With hydrogen; triethylamine; palladium 10% on activated carbon; In methanol; for 24h; under 2585.81 Torr; Product distribution / selectivity;

Reference yield:

phenylmethyl (2S)-2-[({[(1,1-dimethylethyl)oxy]carbonyl}amino)methyl]-4-morpholinecarboxylate (956010-38-1) → tert-butyl N-[[(2S)-morpholin-2-yl]methyl]carbamate (875551-59-0)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; Product distribution / selectivity;

upstream raw materials:

1,1-dimethylethyl ({(2S)-4-[(3,4-dichlorophenyl)methyl]-2-morpholinyl}methyl)carbamate

phenylmethyl (2S)-2-[({[(1,1-dimethylethyl)oxy]carbonyl}amino)methyl]-4-morpholinecarboxylate

1,1-dimethylethyl {[(2R)-4-(phenylmethyl)-2-morpholinyl]methyl}carbamate

Downstream raw materials:

phenylmethyl (2S)-2-[({[(1,1-dimethylethyl)oxy]carbonyl}amino)methyl]-4-morpholinecarboxylate

1,1-dimethylethyl ({(2R)-4-[(2-cyanophenyl)sulfonyl]-2-morpholinyl}methyl)carbamate

N₁-({(2R)-4-[(2-cyanophenyl)sulfonyl]-2-morpholinyl}methyl)-L-leucinamide hydrochloride

N₁-({(2R)-4-[(2-cyanophenyl)sulfonyl]-2-morpholinyl}methyl)-N₂-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide

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