9,10-Dihydrophenanthrene-9,10-diol

Base Information

Chemical Name:9,10-Dihydrophenanthrene-9,10-diol
CAS No.:25061-77-2
Molecular Formula:C14H12 O2
Molecular Weight:212.248
Hs Code.:2906299090
NSC Number:249833
DSSTox Substance ID:DTXSID301297261
Nikkaji Number:J69.565C
Wikidata:Q27117153
Mol file:25061-77-2.mol

Synonyms:9,10-dihydroxy-9,10-dihydrophenanthrene;9,10-dihydroxy-9,10-dihydrophenanthrene, (9R-trans)-isomer;9,10-dihydroxy-9,10-dihydrophenanthrene, (9S-trans)-isomer;9,10-dihydroxy-9,10-dihydrophenanthrene, (cis)-isomer;9,10-dihydroxy-9,10-dihydrophenanthrene, (trans)-isomer;9,10-dihydroxy-9,10-dihydrophenanthrene, trans-(+-)-isomer

Suppliers and Price of 9,10-Dihydrophenanthrene-9,10-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 9,10-Dihydrophenanthrene-9,10-diol

Chemical Property:

Vapor Pressure:2.85E-07mmHg at 25°C
Boiling Point:404.6°Cat760mmHg
Flash Point:200.5°C
PSA：40.46000
Density:1.326g/cm³
LogP:2.43400
XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:212.083729621
Heavy Atom Count:16
Complexity:227

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(C(C3=CC=CC=C32)O)O

Technology Process of 9,10-Dihydrophenanthrene-9,10-diol

There total 2 articles about 9,10-Dihydrophenanthrene-9,10-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-01-8
phenanthrene

: 85-44-9
phthalic anhydride

: 2005-10-9
6H-benzo[c]chromen-6-one

: 5343-99-7
1,2-naphthalenedicarboxylic anhydride

: 486-25-9,952573-42-1
9-fluorenone

: 6050-13-1
biphenyl-2,2'-dicarboxylic acid anhydride

: 569-15-3
1,4-phenanthrenequinone

: 25061-77-2
9,10-dihydrophenanthrene-9,10-diol

: 57404-53-2
1-hydroxyphenanthrenequinone

: 84-11-7
9,10-phenanthrenequinone

: 1210-05-5
Biphenyl-2,2'-dicarbaldehyde

Guidance literature:: phenanthrene; With water; In acetone; for 2h; Darkness;

In acetone; for 1h; Irradiation;
DOI:10.1016/j.molcata.2010.03.029

Reference yield:

: 776-35-2
9,10-dihydrophenanthrene

: 25061-77-2
9,10-dihydrophenanthrene-9,10-diol

: 84-11-7
9,10-phenanthrenequinone

Guidance literature:: With hydrotris(3,4,5-tribromo)pyrazolylborate Cu(NCMe); dihydrogen peroxide; In water; acetonitrile; at 20 ℃; for 2h;
DOI:10.1021/ja310866k

Reference yield: 99.0%

: 673-32-5
1-Phenylprop-1-yne

: 25061-77-2
9,10-dihydrophenanthrene-9,10-diol

: (E)-10-hydroxy-10-(1-phenylprop-1-en-2-yl)phenanthren-9(10H)-one

Guidance literature:: With dodecacarbonyl-triangulo-triruthenium; 1-Adamantanecarboxylic acid; tricyclohexylphosphine; In m-xylene; at 130 ℃; for 4h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201311130