3,3'-Diindolyl-2,2'-tetrasulfide

Base Information

• Chemical Name: 3,3'-Diindolyl-2,2'-tetrasulfide
• CAS No.: 13839-92-4
• Molecular Formula: C₁₆H₁₀N₂S₄
• Molecular Weight: 358.533
• Mol file: 13839-92-4.mol

Synonyms:3,3’-Diindolyl-2,2’-tetrasulfide

Chemical Property of 3,3'-Diindolyl-2,2'-tetrasulfide

Chemical Property:

• Boiling Point: 748.7°Cat760mmHg
• Flash Point: 406.6°C
• PSA: 144.54000
• Density: 1.598g/cm³
• LogP: 6.88820

Purity/Quality:

99%min ^*data from raw suppliers

3,3'-DIINDOLYL-2,2'-TETRASULFIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3'-Diindolyl-2,2'-tetrasulfide

There total 5 articles about 3,3'-Diindolyl-2,2'-tetrasulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

1H,1'H-[3,3']biindolyl (13637-37-1) → 5,10-dihydro[1,2,3,4]tetrathiocino[5,6-b:8,7-b']diindole (13839-92-4)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide; for 48h; Heating;

DOI:10.1039/b109840c

Reference yield:

indole (120-72-9) → 5,10-dihydro[1,2,3,4]tetrathiocino[5,6-b:8,7-b']diindole (13839-92-4)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide; at 145 ℃; for 3h;

DOI:10.1021/ja01496a022

Reference yield:

S,S'-Bis-(3-indolyl)disulphide (61830-39-5) → 5,10-dihydro[1,2,3,4]tetrathiocino[5,6-b:8,7-b']diindole (13839-92-4)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide; at 120 - 130 ℃; for 1.25h;

DOI:10.1021/ja01496a022

upstream raw materials:

indole

S,S'-Bis-(3-indolyl)disulphide

1H,1'H-[3,3']biindolyl

Downstream raw materials:

indolin-2-thione

Refernces