4-tert-butylcyclohexyl benzoate

Base Information

• Chemical Name: 4-tert-butylcyclohexyl benzoate
• CAS No.: 5452-03-9
• Molecular Formula: C₁₇H₂₄O₂
• Molecular Weight: 260.376
• Mol file: 5452-03-9.mol

Synonyms:Cyclohexanol,4-(1,1-dimethylethyl)-, benzoate (9CI); 4-tert-Butylcyclohexyl benzoate; NSC21892

Chemical Property of 4-tert-butylcyclohexyl benzoate

Chemical Property:

• Vapor Pressure: 8.15E-05mmHg at 25°C
• Boiling Point: 341.2°Cat760mmHg
• Flash Point: 155°C
• Density: 1.01g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-tert-butylcyclohexyl benzoate

There total 17 articles about 4-tert-butylcyclohexyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(4-tert-Butyl-cyclohexyloxymethyl)-benzene → trans-4-t-butylcyclohexyl benzoate (170303-74-9,5452-03-9)

Guidance literature:

With potassium carbonate; 1-(tert-butylperoxy)-1,2-benziodoxol-3(1H)-one; In benzene; for 33h; Ambient temperature;

DOI:10.1021/ja9610287

Reference yield: 79.0%

trans-4-tert-butylmesyloxycyclohexane (18508-90-2) + cesium benzoate (17265-04-2) → cis-4-t-butylcyclohexyl benzoate (15867-50-2,5452-03-9)

Guidance literature:

With dmap; In toluene; for 48h; Heating;

DOI:10.1021/jo0007783

Reference yield: 70.0%

(4-tert-Butyl-cyclohexyloxymethyl)-benzene → cis-4-t-butylcyclohexyl benzoate (15867-50-2,5452-03-9)

Guidance literature:

With potassium carbonate; 1-(tert-butylperoxy)-1,2-benziodoxol-3(1H)-one; In benzene; for 36h; Ambient temperature;

DOI:10.1021/ja9610287

upstream raw materials:

Potassium benzoate

trans-4-tert-butylcyclohexanol

cis-4-tert-butyl-1-cyclohexanol

trans-4-tert-butylmesyloxycyclohexane