CID 6330562

Base Information

Chemical Name:CID 6330562
CAS No.:37718-79-9
Molecular Formula:C₂₄H₂₁ClGe₂
Molecular Weight:490.064
Hs Code.:
NSC Number:371173
Mol file:37718-79-9.mol

Synonyms:NSC371173;NSC-371173;37718-79-9

Suppliers and Price of CID 6330562

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of CID 6330562

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:489.9764319
Heavy Atom Count:27
Complexity:331

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[GeH]C2=CC=CC=C2.C1=CC=C(C=C1)[Ge](C2=CC=CC=C2)Cl

Technology Process of CID 6330562

There total 3 articles about CID 6330562 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 128-09-6
N-chloro-succinimide

: 13891-99-1
1,1,2,2-tetraphenyl 1,2-digermane

: 37718-79-9
(C₆H₅)2GeHGeCl(C₆H₅)2

Guidance literature:: In tetrahydrofuran; addn. of chlorosuccinimide to Ge-compound soln., stirring at room temp. for 16 h (inert atmosphere); evpan., extn. (ether-pentane 4:1), concn., standing at -30°C for 12 h, pptn., drying (vac.); elem. anal.;
DOI:10.1016/0022-328X(93)80281-F

Reference yield: 52.0%

: 7366-23-6
diphenylchlorogermane

: 6674-22-2,83329-50-4
1,8-diazabicyclo[5.4.0]undec-7-ene

: 37718-79-9
(C₆H₅)2GeHGeCl(C₆H₅)2

Guidance literature:: In benzene; 20°C;;
DOI:10.1016/0022-328X(85)87439-8

Reference yield: 21.0%

: 623-73-4
diazoacetic acid ethyl ester

: 7366-23-6
diphenylchlorogermane

: 37718-79-9
(C₆H₅)2GeHGeCl(C₆H₅)2

: 83686-70-8
Ge(C₆H₅)2ClCH₂COOCH₂CH₃

Guidance literature:: In neat (no solvent); byproducts: ClCH2COOCH2CH3; diazoacetate adding to germane and heating for 12 h at 60°C; identified by NMR spectrum;
DOI:10.1016/S0022-328X(00)87639-1