Glycine, N-[(1S,2S)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]cyclohexyl]- N-[(2R)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]-3-(4-nitrophenyl )propyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Glycine, N-[(1S,2S)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]cyclohexyl]- N-[(2R)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]-3-(4-nitrophenyl )propyl]-, 1,1-dimethylethyl ester
CAS No.:880644-82-6
Molecular Formula:C45H74N4O12
Molecular Weight:863.102
Hs Code.:

Glycine,
N-[(1S,2S)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]cyclohexyl]-
N-[(2R)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]-3-(4-nitrophenyl
)propyl]-, 1,1-dimethylethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Glycine, N-[(1S,2S)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]cyclohexyl]- N-[(2R)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]-3-(4-nitrophenyl )propyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Glycine, N-[(1S,2S)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]cyclohexyl]- N-[(2R)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]-3-(4-nitrophenyl )propyl]-, 1,1-dimethylethyl ester

There total 1 articles about Glycine, N-[(1S,2S)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]cyclohexyl]- N-[(2R)-2-[bis[2-(1,1-dimethylethoxy)-2-oxoethyl]amino]-3-(4-nitrophenyl )propyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: N-[(R)-2-amino-3-(p-nitrophenyl)propyl]-trans-(S,S)-cyclohexane-1,2-diamine trihydrochloride

: 880644-82-6
N-[(R)-2-amino-3-(p-nitrophenyl)propyl]-trans-(S,S)-cyclohexane-1,2-diamine-N,N,N',N'',N''-penta-tert-butyl acetate

Guidance literature:: With K₂O₃; In acetonitrile; for 72h;
DOI:10.1021/jm060317v

Reference yield: 97.0%

: 880644-82-6
N-[(R)-2-amino-3-(p-nitrophenyl)propyl]-trans-(S,S)-cyclohexane-1,2-diamine-N,N,N',N'',N''-penta-tert-butyl acetate

: 880644-84-8
N-[(R)-2-amino-3-(p-aminophenyl)propyl]-trans-(S,S)-cyclohexane-1,2-diamine-N,N,N',N'',N''-penta-tert-butyl acetate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 8h; atmospheric pressure;
DOI:10.1021/jm060317v

Reference yield:

: 880644-82-6
N-[(R)-2-amino-3-(p-nitrophenyl)propyl]-trans-(S,S)-cyclohexane-1,2-diamine-N,N,N',N'',N''-penta-tert-butyl acetate

: 905825-53-8
N-[(R)-2-amino-3-(p-aminophenyl-N-{5-oxopentanoic acid})-propyl]-trans-(S,S)-cyclohexane-1,2-diamine-N,N,N',N'',N''-penta-tert-butyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / H₂ / Pd/C / ethanol / 8 h / atmospheric pressure

2: 71 percent / benzene

With hydrogen; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1021/jm060317v