1H-Benzimidazole-1-acetic acid, 5-[(phenylmethyl)amino]-2-propyl-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: 1H-Benzimidazole-1-acetic acid, 5-[(phenylmethyl)amino]-2-propyl-, 1,1-dimethylethyl ester
• CAS No.: 881427-77-6
• Molecular Formula: C23H29N3O2
• Molecular Weight: 379.502

Synonyms:

Chemical Property of 1H-Benzimidazole-1-acetic acid, 5-[(phenylmethyl)amino]-2-propyl-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 1H-Benzimidazole-1-acetic acid, 5-[(phenylmethyl)amino]-2-propyl-, 1,1-dimethylethyl ester

There total 1 articles about 1H-Benzimidazole-1-acetic acid, 5-[(phenylmethyl)amino]-2-propyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5-amino-2-propylbenzoimidazol-1-yl)acetic acid tert-butyl ester (881427-36-7) + benzaldehyde (100-52-7) → (5-benzylamino-2-propylbenzoimidazol-1-yl)acetic acid tert-butyl ester (881427-77-6)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;

Reference yield:

(5-benzylamino-2-propylbenzoimidazol-1-yl)acetic acid tert-butyl ester (881427-77-6) + acetyl chloride (75-36-5) → [5-(acetylbenzylamino)-2-propylbenzoimidazol-1-yl]acetic acid tert-butyl ester (881427-78-7)

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

2-Thiophenecarbonyl chloride (5271-67-0) + (5-benzylamino-2-propylbenzoimidazol-1-yl)acetic acid tert-butyl ester (881427-77-6) → {5-[benzyl-(thiophene-2-carbonyl)amino]-2-propylbenzoimidazol-1-yl}acetic acid tert-butyl ester (881428-06-4)

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

upstream raw materials:

(5-amino-2-propylbenzoimidazol-1-yl)acetic acid tert-butyl ester

benzaldehyde

Downstream raw materials:

[5-(acetylbenzylamino)-2-propylbenzoimidazol-1-yl]acetic acid tert-butyl ester

{5-[benzyl-(thiophene-2-carbonyl)amino]-2-propylbenzoimidazol-1-yl}acetic acid tert-butyl ester

{5-[benzyl-(4-chlorobenzoyl)amino]-2-propylbenzoimidazol-1-yl}acetic acid tert-butyl ester

{5-[benzyl-(4-fluorobenzoyl)amino]-2-propylbenzoimidazol-1-yl}acetic acid tert-butyl ester

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