Phenol, 3-[(1S)-1-(methylamino)ethyl]-

Base Information

Chemical Name:Phenol, 3-[(1S)-1-(methylamino)ethyl]-
CAS No.:894079-42-6
Molecular Formula:C9H13NO
Molecular Weight:151.208
Hs Code.:
European Community (EC) Number:805-518-8
DSSTox Substance ID:DTXSID90467567
Nikkaji Number:J3.042.912E
Wikidata:Q82294568

Synonyms:Phenol, 3-[(1S)-1-(methylamino)ethyl]-;894079-42-6;(S)-3-(1-(Methylamino)ethyl)phenol;3-[(1S)-1-(methylamino)ethyl]phenol;3-((1S)-1-(Methylamino)ethyl)phenol;EC 805-518-8;SCHEMBL414424;DTXSID90467567;CS-0459291

Suppliers and Price of Phenol, 3-[(1S)-1-(methylamino)ethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Phenol, 3-[(1S)-1-(methylamino)ethyl]-

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:151.099714038
Heavy Atom Count:11
Complexity:116

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1=CC(=CC=C1)O)NC
Isomeric SMILES:C[C@@H](C1=CC(=CC=C1)O)NC

Technology Process of Phenol, 3-[(1S)-1-(methylamino)ethyl]-

There total 8 articles about Phenol, 3-[(1S)-1-(methylamino)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1017234-23-9
(1S)-N-((S)-1-(3-hydroxyphenyl)ethyl)-N-methyl-1-phenylethanamine

: 894079-42-6
3-[(S)-1-(methylamino)ethyl]phenol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 16h; under 3878.71 Torr; regioselective reaction; Inert atmosphere;
DOI:10.1080/00397911.2010.527425

Reference yield: 45.0%

: 923035-06-7
3-((1-methylamino)ethyl)phenol

: 894079-42-6
3-[(S)-1-(methylamino)ethyl]phenol

Guidance literature:: With D-tartaric acid; In isopropyl alcohol; at 40 - 50 ℃; for 2.5h; Reagent/catalyst; Solvent; Temperature; Reflux;

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 894079-42-6
3-[(S)-1-(methylamino)ethyl]phenol

Guidance literature:: Multi-step reaction with 4 steps

1: titanium(IV) isopropylate / ethyl acetate / 3 h / Inert atmosphere

2: sodium tetrahydroborate / ethanol; ethyl acetate / 3 h / 0 °C / Inert atmosphere

3: formic acid / water / 10 h / 70 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 3878.71 Torr / Inert atmosphere

With titanium(IV) isopropylate; sodium tetrahydroborate; formic acid; palladium 10% on activated carbon; hydrogen; In ethanol; water; ethyl acetate;
DOI:10.1080/00397911.2010.527425