Tricyclo(3.3.1.1(3,7))decan-1-amine, N-(1-methylethyl)-

Base Information

• Chemical Name: Tricyclo(3.3.1.1(3,7))decan-1-amine, N-(1-methylethyl)-
• CAS No.: 3667-90-1
• Molecular Formula: C13H23N
• Molecular Weight: 193.3284
• DSSTox Substance ID: DTXSID50190122
• Wikidata: Q83062407
• Mol file: 3667-90-1.mol

Synonyms:N-isopropyladamantan-1-amine;Tricyclo(3.3.1.1(3,7))decan-1-amine, N-(1-methylethyl)-;3667-90-1;N-(1-Methylethyl)tricyclo(3.3.1.1(3,7))decan-1-amine;SCHEMBL105165;DTXSID50190122;FSMRLILYPRGBDS-UHFFFAOYSA-N;Tricyclo[3.3.1.1]decan-1-amine, N-(1-methylethyl)-

Chemical Property of Tricyclo(3.3.1.1(3,7))decan-1-amine, N-(1-methylethyl)-

Chemical Property:

• Vapor Pressure: 0.025mmHg at 25°C
• Boiling Point: 247.9°Cat760mmHg
• Flash Point: 98.2°C
• Density: 0.97g/cm³
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 193.183049738
• Heavy Atom Count: 14
• Complexity: 190

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)NC12CC3CC(C1)CC(C3)C2

Technology Process of Tricyclo(3.3.1.1(3,7))decan-1-amine, N-(1-methylethyl)-

There total 5 articles about Tricyclo(3.3.1.1(3,7))decan-1-amine, N-(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1-Adamantanamine (768-94-5) + diisopropylamine (108-18-9) → i-propyladamantylamine (3667-90-1)

Guidance literature:

With μ-diiodo-di((η5-pentamethylcyclopentadienyl)(iodo)iridium); In 5,5-dimethyl-1,3-cyclohexadiene; at 155 ℃; for 10h; Inert atmosphere;

DOI:10.1002/anie.200904028

Reference yield:

1-Adamantanamine (768-94-5) + isopropyl alcohol (67-63-0,8013-70-5) → i-propyladamantylamine (3667-90-1)

Guidance literature:

With Cu/Al₂O₃; hydrogen; In o-xylene; at 200 ℃; for 6h; under 3750.38 - 30003 Torr; Autoclave;

Reference yield:

1-Adamantyl bromide (768-90-1) + isopropylamine (75-31-0) → i-propyladamantylamine (3667-90-1)

Guidance literature:

at 215 ℃;

DOI:10.1021/jm00288a019

upstream raw materials:

1-Adamantyl bromide

isopropylamine

1-Adamantanamine

diisopropylamine