Pyrazinecarbonitrile, 5-phenyl-

Base Information

Chemical Name:Pyrazinecarbonitrile, 5-phenyl-
CAS No.:90687-96-0
Molecular Formula:C11H7N3
Molecular Weight:181.197
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyrazinecarbonitrile, 5-phenyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Pyrazinecarbonitrile, 5-phenyl-

There total 3 articles about Pyrazinecarbonitrile, 5-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 90687-94-8
6-Phenyl-2-pyrazinecarboxamide

: 90687-96-0
5-Phenyl-2-pyrazinecarbonitrile

Guidance literature:: With trichlorophosphate; Heating;

Reference yield: 66.0%

: 7677-24-9
trimethylsilyl cyanide

: 29460-97-7
2-phenylpyrazine

: 2882-16-8
3-phenylpyrazine-2-carbonitrile

: 90687-96-0
5-Phenyl-2-pyrazinecarbonitrile

: 90701-04-5
6-Phenyl-2-pyrazinecarbonitrile

Guidance literature:: 2-phenylpyrazine; With trifluoromethylsulfonic anhydride; In chloroform; at 20 ℃; for 1h; Inert atmosphere; Sealed tube;

trimethylsilyl cyanide; In chloroform; at 60 ℃; for 3h; Inert atmosphere; Sealed tube;

With 4-methyl-morpholine; In chloroform; at 60 ℃; for 17h; Overall yield = 80 %; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201703931

Reference yield: 17.0%

: 19847-12-2
2-pyrazine carbonitrile

: 98-80-6
phenylboronic acid

: 2882-16-8
3-phenylpyrazine-2-carbonitrile

: 90687-96-0
5-Phenyl-2-pyrazinecarbonitrile

: 90701-04-5
6-Phenyl-2-pyrazinecarbonitrile

Guidance literature:: 2-pyrazine carbonitrile; phenylboronic acid; With Selectfluor; trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 0.0166667h;

With silver nitrate; In dichloromethane; water; at 50 ℃;
DOI:10.1021/acs.orglett.7b02706