Germane, chlorotris(2-methyl-2-phenylpropyl)-

Base Information

Chemical Name:Germane, chlorotris(2-methyl-2-phenylpropyl)-
CAS No.:90753-11-0
Molecular Formula:C₃₀H₃₉ClGe
Molecular Weight:507.683
Hs Code.:

Synonyms:

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Chemical Property of Germane, chlorotris(2-methyl-2-phenylpropyl)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Germane, chlorotris(2-methyl-2-phenylpropyl)-

There total 1 articles about Germane, chlorotris(2-methyl-2-phenylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 10038-98-9
germaniumtetrachloride

: 35293-35-7
2-methyl-2-phenyl-1-propylmagnesium chloride

: 90753-11-0
(C₆H₅C(CH₃)2CH₂)3GeCl

Guidance literature:: In tetrahydrofuran; benzene; byproducts: t-butylbenzene; an excess of Grignard reagent soln. in THF and GeCl4 soln. in benzene mixing and refluxing for 12 h, hydrolyzing, volatiles removing by vacuum distillation; identified by elem. anal., NMR and mass spectra;
DOI:10.1016/0022-328X(84)85144-X

Reference yield: 96.6%

: 90753-11-0
(C₆H₅C(CH₃)2CH₂)3GeCl

: 90753-12-1
(C₆H₅C(CH₃)2CH₂)3GeH

Guidance literature:: In diethyl ether; chlorogermane to a susp. of LiAlH4 in ether adding, refluxing for 1 h, hydrolyzing; purified after usual work-up by recrystallization from hexane, identified by elem. anal., IR, NMR and mass spectra;
DOI:10.1016/0022-328X(84)85144-X

Reference yield: 13.0%

: 90753-11-0
(C₆H₅C(CH₃)2CH₂)3GeCl

: 1911-01-9
1,1',3,3'-tetramethyl-2,2'-biimidazolidinylidene

: hexaneophyldigermane

: 37091-73-9
2-chloro-1,3-dimethylimidazolinium chloride

Guidance literature:: In toluene; Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at room temp., MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, NMR and mass spectra;
DOI:10.1016/0022-328X(84)85144-X