3-AMINO-3-(4-METHYLPHENYL)-2-PROPENOIC ACID ETHYL ESTER

Base Information

Chemical Name:3-AMINO-3-(4-METHYLPHENYL)-2-PROPENOIC ACID ETHYL ESTER
CAS No.:91108-05-3
Molecular Formula:C12H15NO2
Molecular Weight:205.257
Hs Code.:
Mol file:91108-05-3.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-AMINO-3-(4-METHYLPHENYL)-2-PROPENOIC ACID ETHYL ESTER

Chemical Property:

PSA：52.32000
LogP:2.55800

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:

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Technology Process of 3-AMINO-3-(4-METHYLPHENYL)-2-PROPENOIC ACID ETHYL ESTER

There total 2 articles about 3-AMINO-3-(4-METHYLPHENYL)-2-PROPENOIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 27835-00-3
ethyl (4-methylbenzoyl)acetate

: 91108-05-3
ethyl 3-amino-3-(p-tolyl)-2-propenoate

Guidance literature:: With ammonium acetate; In ethanol;
DOI:10.1002/adsc.201501061

Reference yield:

: 105-36-2
ethyl bromoacetate

: 104-85-8
para-methylbenzonitrile

: 91108-05-3
ethyl 3-amino-3-(p-tolyl)-2-propenoate

Guidance literature:: ethyl bromoacetate; para-methylbenzonitrile; With methanesulfonic acid; zinc; In tetrahydrofuran; for 3h; Reflux; Inert atmosphere;

With water; potassium carbonate; In ethyl acetate; for 0.5h;
DOI:10.1002/ejoc.201701472

Reference yield: 90.0%

: 2314-97-8,263005-66-9
iodotrifluoromethane

: 91108-05-3
ethyl 3-amino-3-(p-tolyl)-2-propenoate

: 1365265-06-0
ethyl 3-oxo-3-(p-tolyl)-2-(trifluoromethyl)propionate

Guidance literature:: iodotrifluoromethane; ethyl 3-amino-3-(p-tolyl)-2-propenoate; With dihydrogen peroxide; iron(II) sulfate; In water; dimethyl sulfoxide; at 20 ℃; for 1h; Inert atmosphere;

With hydrogenchloride; In water; dimethyl sulfoxide; for 2h;
DOI:10.1016/j.jfluchem.2015.10.013