Digermane, 1,1-diethyl-1-(methylthio)-2,2,2-triphenyl-

Base Information

Chemical Name:Digermane, 1,1-diethyl-1-(methylthio)-2,2,2-triphenyl-
CAS No.:91123-30-7
Molecular Formula:C₂₃H₂₈Ge₂S
Molecular Weight:481.721
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Digermane, 1,1-diethyl-1-(methylthio)-2,2,2-triphenyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Digermane, 1,1-diethyl-1-(methylthio)-2,2,2-triphenyl-

There total 1 articles about Digermane, 1,1-diethyl-1-(methylthio)-2,2,2-triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 624-92-0
Dimethyldisulphide

: 91123-29-4
Ph₃GeGe(Et)2H

: 91123-30-7
(C₆H₅)3GeGe(SCH₃)(CH₂CH₃)2

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In neat (no solvent); Ge deriv. heating with an excess of disulfide and a catalytic amt. of AIBN in a sealed tube for 12 h at 100°C, volatiles removing in vacuo, white crystalline residue washing with pentane; identified by elem. anal. and NMR spectrum;
DOI:10.1016/0022-328X(84)85145-1