3(2H)-Pyridazinone,4-chloro-5-[[1,6-dihydro-1-methyl-6-oxo-5-[(phenylmethyl)amino]-4-pyridazinyl]thio]-2-methyl-

Base Information

Chemical Name:3(2H)-Pyridazinone,4-chloro-5-[[1,6-dihydro-1-methyl-6-oxo-5-[(phenylmethyl)amino]-4-pyridazinyl]thio]-2-methyl-
CAS No.:91364-79-3
Molecular Formula:C17H16ClN5O2S
Molecular Weight:389.865
Hs Code.:

Synonyms:3(2H)-Pyridazinone,4-chloro-5-[[1,6-dihydro-1-methyl-6-oxo-5-[(phenylmethyl)amino]-4-pyridazinyl]thio]-2-methyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3(2H)-Pyridazinone,4-chloro-5-[[1,6-dihydro-1-methyl-6-oxo-5-[(phenylmethyl)amino]-4-pyridazinyl]thio]-2-methyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3(2H)-Pyridazinone,4-chloro-5-[[1,6-dihydro-1-methyl-6-oxo-5-[(phenylmethyl)amino]-4-pyridazinyl]thio]-2-methyl-

There total 2 articles about 3(2H)-Pyridazinone,4-chloro-5-[[1,6-dihydro-1-methyl-6-oxo-5-[(phenylmethyl)amino]-4-pyridazinyl]thio]-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 933-76-6
4,5-dichloro-2-methyl-3(2H)-pyridazinone

: 91736-91-3
2-methyl-4-benzylamino-5-mercapto-3(2H)-pyridazinone

: 91364-79-3
5-(2-methyl-4-benzylamino-2,3-dihydro-3-oxo-pyridazinyl) 5'-(2'-methyl-4'-chloro-2',3'-dihydro-3'-oxo-pyridazinyl) sulfide

Guidance literature:: With potassium hydroxide; In methanol; N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 91736-88-8
4-(N-benzylamino)-5-chloro-2-methyl-3(2H)-pyridazinone

: 91364-79-3
5-(2-methyl-4-benzylamino-2,3-dihydro-3-oxo-pyridazinyl) 5'-(2'-methyl-4'-chloro-2',3'-dihydro-3'-oxo-pyridazinyl) sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / 70 percent sodium hydrosulfide / dimethylformamide / 10 h / 90 °C

2: 52 percent / KOH / dimethylformamide; methanol / 1 h / Ambient temperature

With potassium hydroxide; sodium hydrogensulfide; In methanol; N,N-dimethyl-formamide;