4-(Benzylamino)-2-methyl-5-sulfanylpyridazin-3-one

Base Information

Chemical Name:4-(Benzylamino)-2-methyl-5-sulfanylpyridazin-3-one
CAS No.:91736-91-3
Molecular Formula:C12H13N3OS
Molecular Weight:247.321
Hs Code.:
DSSTox Substance ID:DTXSID901179352

Synonyms:91736-91-3;DTXSID901179352;5-Mercapto-2-methyl-4-[(phenylmethyl)amino]-3(2H)-pyridazinone

Suppliers and Price of 4-(Benzylamino)-2-methyl-5-sulfanylpyridazin-3-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(Benzylamino)-2-methyl-5-sulfanylpyridazin-3-one

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:247.07793322
Heavy Atom Count:17
Complexity:359

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=O)C(=C(C=N1)S)NCC2=CC=CC=C2

Technology Process of 4-(Benzylamino)-2-methyl-5-sulfanylpyridazin-3-one

There total 1 articles about 4-(Benzylamino)-2-methyl-5-sulfanylpyridazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 91736-88-8
4-(N-benzylamino)-5-chloro-2-methyl-3(2H)-pyridazinone

: 91736-91-3
2-methyl-4-benzylamino-5-mercapto-3(2H)-pyridazinone

Guidance literature:: With sodium hydrogensulfide; In N,N-dimethyl-formamide; at 90 ℃; for 10h;

Reference yield: 52.0%

: 933-76-6
4,5-dichloro-2-methyl-3(2H)-pyridazinone

: 91736-91-3
2-methyl-4-benzylamino-5-mercapto-3(2H)-pyridazinone

: 91364-79-3
5-(2-methyl-4-benzylamino-2,3-dihydro-3-oxo-pyridazinyl) 5'-(2'-methyl-4'-chloro-2',3'-dihydro-3'-oxo-pyridazinyl) sulfide

Guidance literature:: With potassium hydroxide; In methanol; N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 91736-91-3
2-methyl-4-benzylamino-5-mercapto-3(2H)-pyridazinone

: 87633-85-0
10-benzyl-2,7-dimethyl-10H-dipyridazino<4,5-b:4',5'-e><1,4>thiazine-1,6(2H,7H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / KOH / dimethylformamide; methanol / 1 h / Ambient temperature

2: 79 percent / 10 percent aq. NaOH / 2 h / 120 °C

With potassium hydroxide; sodium hydroxide; In methanol; N,N-dimethyl-formamide;