4-Hydroxy-3-methoxybenzoic acid hexyl ester

Base Information

• Chemical Name: 4-Hydroxy-3-methoxybenzoic acid hexyl ester
• CAS No.: 84375-71-3
• Molecular Formula: C14H20O4
• Molecular Weight: 252.31
• Mol file: 84375-71-3.mol

Synonyms:Hexyl vanillate;Vanillinsaeure-hexylester;n-hexyl vanillate;4-Hydroxy-3-methoxy-benzoesaeure-hexylester;4-Hydroxy-3-methoxybenzoic acid hexyl ester;

Chemical Property of 4-Hydroxy-3-methoxybenzoic acid hexyl ester

Chemical Property:

• Vapor Pressure: 4.98E-06mmHg at 25°C
• Boiling Point: 371°Cat760mmHg
• Flash Point: 133°C
• PSA: 55.76000
• Density: 1.086g/cm³
• LogP: 3.13790

Purity/Quality:

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 4-Hydroxy-3-methoxybenzoic acid hexyl ester

There total 1 articles about 4-Hydroxy-3-methoxybenzoic acid hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

3-methoxy-4-hydroxybenzoic acid (121-34-6) + hexan-1-ol (111-27-3) → n-hexyl 4-hydroxy-3-methoxybenzoate (84375-71-3)

Guidance literature:

With toluene-4-sulfonic acid; mercury; In toluene;

Reference yield:

2-chloropyridine (109-09-1) + carbon monoxide (201230-82-2) + n-hexyl 4-hydroxy-3-methoxybenzoate (84375-71-3) → pyridine-2-carboxylic acid 4-hexyloxycarbonyl-2-methoxy-phenyl ester

Guidance literature:

With bis(benzonitrile)palladium(II) dichloride; 1,3-bis-(diphenylphosphino)propane; triethylamine; In N,N-dimethyl-formamide; at 130 ℃; for 14h; under 18751.5 Torr;

DOI:10.1021/jo034112v

upstream raw materials:

3-methoxy-4-hydroxybenzoic acid

hexan-1-ol

Refernces

• 1、 -. "Vanillic acid ester perfuming agents". . . Retrieved 2008/06/13.