3-iodo-N,N-dimethylbenzamide

Base Information

Chemical Name:3-iodo-N,N-dimethylbenzamide
CAS No.:91506-06-8
Molecular Formula:C9H10INO
Molecular Weight:275.089
Hs Code.:
DSSTox Substance ID:DTXSID301308983
Nikkaji Number:J1.831.985C

Synonyms:3-iodo-N,N-dimethylbenzamide;91506-06-8;N,N-Dimethyl-3-iodobenzamide;SCHEMBL2086375;XSLDOPYONMGECY-UHFFFAOYSA-N;DTXSID301308983;AKOS003635184;CS-0197504;FT-0765726;E73986;Z32014543

Suppliers and Price of 3-iodo-N,N-dimethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-iodo-N,N-dimethylbenzamide

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:274.98071
Heavy Atom Count:12
Complexity:170

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)C(=O)C1=CC(=CC=C1)I

Technology Process of 3-iodo-N,N-dimethylbenzamide

There total 4 articles about 3-iodo-N,N-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 618-51-9
3-Iodobenzoic acid

: 91506-06-8
N,N-dimethyl-3-iodobenzamide

Guidance literature:: With di-tert-butyl peroxide; copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 130 ℃; for 12h; Sealed tube;
DOI:10.1016/j.cclet.2014.09.007

Reference yield:

: 124-40-3
dimethyl amine

: 618-51-9
3-Iodobenzoic acid

: 91506-06-8
N,N-dimethyl-3-iodobenzamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; for 18h;

Reference yield:

: 618-51-9
3-Iodobenzoic acid

: 91506-06-8
N,N-dimethyl-3-iodobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 2 h / Heating

2: H₂O / 0.5 h / Ambient temperature

With thionyl chloride; In water;
DOI:10.1039/p19960001927