4,7-Phenanthroline, 3,8-bis[5-(4-methoxyphenyl)-2-pyridinyl]-

Base Information

Chemical Name:4,7-Phenanthroline, 3,8-bis[5-(4-methoxyphenyl)-2-pyridinyl]-
CAS No.:915283-62-4
Molecular Formula:C36H26N4O2
Molecular Weight:546.628
Hs Code.:

Synonyms:4,7-Phenanthroline,3,8-bis[5-(4-methoxyphenyl)-2-pyridinyl];3,8-bis(4'-(4-methoxyphenyl)-2'-pyridyl)-4,7-phenanthroline;

Suppliers and Price of 4,7-Phenanthroline, 3,8-bis[5-(4-methoxyphenyl)-2-pyridinyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,7-Phenanthroline, 3,8-bis[5-(4-methoxyphenyl)-2-pyridinyl]-

Chemical Property:

PSA：70.02000
LogP:8.25820

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,7-Phenanthroline, 3,8-bis[5-(4-methoxyphenyl)-2-pyridinyl]-

There total 3 articles about 4,7-Phenanthroline, 3,8-bis[5-(4-methoxyphenyl)-2-pyridinyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3,8-bis(4-bromo-2'-pyridyl)-4,7-phenanthroline

: 5720-07-0
4-methoxyphenylboronic acid

: 915283-62-4
3,8-bis(4'-(4-methoxyphenyl)-2'-pyridyl)-4,7-phenanthroline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 21h; Inert atmosphere;
DOI:10.1021/ja801924y

Reference yield:

: 199867-78-2
3,8-Dibromo-4,7-phenanthroline

: 915283-62-4
3,8-bis(4'-(4-methoxyphenyl)-2'-pyridyl)-4,7-phenanthroline

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Pd(PPh₃)4 / toluene / 62 h / 140 °C

2: 64 percent / potassium carbonate; Pd(PPh₃)4 / dimethylformamide / 21 h / 120 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In N,N-dimethyl-formamide; toluene; 1: Stille coupling / 2: Suzuki coupling;
DOI:10.1039/b601703g

Reference yield:

: 198985-48-7
5-bromo-2-(trimethylstannyl)pyridine

: 915283-62-4
3,8-bis(4'-(4-methoxyphenyl)-2'-pyridyl)-4,7-phenanthroline

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Pd(PPh₃)4 / toluene / 62 h / 140 °C

2: 64 percent / potassium carbonate; Pd(PPh₃)4 / dimethylformamide / 21 h / 120 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In N,N-dimethyl-formamide; toluene; 1: Stille coupling / 2: Suzuki coupling;
DOI:10.1039/b601703g