Carbamic acid, N-[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl]-N-[2-[( 2-phenylacetyl)amino]ethyl]-, 4-(hydroxymethyl)phenyl ester

Base Information

Chemical Name:Carbamic acid, N-[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl]-N-[2-[( 2-phenylacetyl)amino]ethyl]-, 4-(hydroxymethyl)phenyl ester
CAS No.:916084-80-5
Molecular Formula:C28H37N3O8
Molecular Weight:543.617
Hs Code.:

Carbamic acid,
N-[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl]-N-[2-[(
2-phenylacetyl)amino]ethyl]-, 4-(hydroxymethyl)phenyl ester

Synonyms:

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Chemical Property of Carbamic acid, N-[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl]-N-[2-[( 2-phenylacetyl)amino]ethyl]-, 4-(hydroxymethyl)phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

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Useful:

Technology Process of Carbamic acid, N-[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl]-N-[2-[( 2-phenylacetyl)amino]ethyl]-, 4-(hydroxymethyl)phenyl ester

There total 6 articles about Carbamic acid, N-[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl]-N-[2-[( 2-phenylacetyl)amino]ethyl]-, 4-(hydroxymethyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 916084-77-0
[2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester

: 916084-80-5
[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamic acid 4-hydroxymethyl-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 250 mg / Et₃N / dimethylformamide

2: TFA

3: 140 mg / Et₃N / dimethylformamide / 0.17 h

With triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200500842

Reference yield:

: 916084-79-2
(2-tert-butoxycarbonylamino-ethyl)-(2-phenylacetylamino-ethyl)-carbamic acid 4-hydroxymethyl-phenyl ester

: 916084-80-5
[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamic acid 4-hydroxymethyl-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA

2: 140 mg / Et₃N / dimethylformamide / 0.17 h

With triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200500842

Reference yield:

: 103-82-2
phenylacetic acid

: 916084-80-5
[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamic acid 4-hydroxymethyl-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran

2: tetrahydrofuran

3: 250 mg / Et₃N / dimethylformamide

4: TFA

5: 140 mg / Et₃N / dimethylformamide / 0.17 h

With triethylamine; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.200500842