Carbonic acid, [4-[[[[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl][2-[(2- phenylacetyl)amino]ethyl]amino]carbonyl]oxy]phenyl]methyl 4-nitrophenyl ester

Base Information

Chemical Name:Carbonic acid, [4-[[[[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl][2-[(2- phenylacetyl)amino]ethyl]amino]carbonyl]oxy]phenyl]methyl 4-nitrophenyl ester
CAS No.:916084-81-6
Molecular Formula:C35H40N4O12
Molecular Weight:708.722
Hs Code.:

Carbonic acid,
[4-[[[[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl][2-[(2-
phenylacetyl)amino]ethyl]amino]carbonyl]oxy]phenyl]methyl
4-nitrophenyl ester

Synonyms:

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Chemical Property of Carbonic acid, [4-[[[[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl][2-[(2- phenylacetyl)amino]ethyl]amino]carbonyl]oxy]phenyl]methyl 4-nitrophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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Useful:

Technology Process of Carbonic acid, [4-[[[[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl][2-[(2- phenylacetyl)amino]ethyl]amino]carbonyl]oxy]phenyl]methyl 4-nitrophenyl ester

There total 7 articles about Carbonic acid, [4-[[[[2-[[[(3-hydroxy-3-methyl-5-oxohexyl)oxy]carbonyl]amino]ethyl][2-[(2- phenylacetyl)amino]ethyl]amino]carbonyl]oxy]phenyl]methyl 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 916084-80-5
[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamic acid 4-hydroxymethyl-phenyl ester

: 7693-46-1
4-Nitrophenyl chloroformate

: 916084-81-6
carbonic acid 4-[[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamoyloxy]-benzyl ester 4-nitro-phenyl ester

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran;
DOI:10.1002/anie.200500842

Reference yield:

: 916084-77-0
[2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester

: 916084-81-6
carbonic acid 4-[[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamoyloxy]-benzyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 250 mg / Et₃N / dimethylformamide

2: TFA

3: 140 mg / Et₃N / dimethylformamide / 0.17 h

4: 25 percent / Et₃N; DMAP / tetrahydrofuran

With dmap; triethylamine; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.200500842

Reference yield:

: (2-amino-ethyl)-(2-phenylacetylamino-ethyl)-carbamic acid 4-hydroxymethyl-phenyl ester

: 916084-81-6
carbonic acid 4-[[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamoyloxy]-benzyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 140 mg / Et₃N / dimethylformamide / 0.17 h

2: 25 percent / Et₃N; DMAP / tetrahydrofuran

With dmap; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.200500842