2-(3,4-Dichlorobenzoyl)aniline

Base Information

Chemical Name:2-(3,4-Dichlorobenzoyl)aniline
CAS No.:91713-52-9
Molecular Formula:C13H9Cl2NO
Molecular Weight:266.127
Hs Code.:
DSSTox Substance ID:DTXSID901259085

Synonyms:2-(3,4-dichlorobenzoyl)aniline;91713-52-9;DTXSID901259085;AKOS013746333;(2-Aminophenyl)(3,4-dichlorophenyl)methanone;(2-aminophenyl)-(3,4-dichlorophenyl)methanone

Suppliers and Price of 2-(3,4-Dichlorobenzoyl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(3,4-Dichlorobenzoyl)aniline

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:265.0061193
Heavy Atom Count:17
Complexity:285

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)C2=CC(=C(C=C2)Cl)Cl)N

Technology Process of 2-(3,4-Dichlorobenzoyl)aniline

There total 3 articles about 2-(3,4-Dichlorobenzoyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 18282-59-2
4-bromo-1,2-dichlorobenzene

: 133776-41-7
anthranilic acid N-methoxy-N-methylamide

: 91713-52-9
(2-aminophenyl)(3,4-dichlorophenyl)methanone

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1021/jm400652r

Reference yield:

: 6574-99-8
3,4-dichloro-benzonitrile

: 62-53-3
aniline

: 91713-52-9
(2-aminophenyl)(3,4-dichlorophenyl)methanone

Guidance literature:: With aluminum (III) chloride; water; boron trichloride; In toluene;
DOI:10.2174/1573406417666210216154428

Reference yield:

: 118-48-9
isatoic anhydride

: 91713-52-9
(2-aminophenyl)(3,4-dichlorophenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / ethanol / 0.17 h

1.2: 2 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

With n-butyllithium; triethylamine; In tetrahydrofuran; ethanol; hexane;
DOI:10.1021/jm400652r