Boranamine, 1,1-dichloro-N-[2,4,6-tris(1,1-dimethylethyl)phenyl]-

Base Information

Chemical Name:Boranamine, 1,1-dichloro-N-[2,4,6-tris(1,1-dimethylethyl)phenyl]-
CAS No.:91915-27-4
Molecular Formula:C₁₈H₃₀BCl₂N
Molecular Weight:342.16
Hs Code.:

Synonyms:

Suppliers and Price of Boranamine, 1,1-dichloro-N-[2,4,6-tris(1,1-dimethylethyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Boranamine, 1,1-dichloro-N-[2,4,6-tris(1,1-dimethylethyl)phenyl]-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Boranamine, 1,1-dichloro-N-[2,4,6-tris(1,1-dimethylethyl)phenyl]-

There total 1 articles about Boranamine, 1,1-dichloro-N-[2,4,6-tris(1,1-dimethylethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 10294-34-5
boron trichloride

: 102745-24-4
2,4,6-tri-t-butylanilidolithium

: 91915-27-4
BCl₂(NHC₆H₂But₃-2,4,6)

Guidance literature:: In hexane; react. 2,4,6-tri-t-butylanilidolithium with BCl3 in n-C6H14 at -78°C, then -4°C for 12 h; product filtered and crystd. at -30°C from concd. filtrate followed by sublimation; elem. anal.;
DOI:10.1039/c39840000662

Reference yield: 80.0%

: 91915-27-4
BCl₂(NHC₆H₂But₃-2,4,6)

: 91915-29-6
B(NH₂)2(NHC₆H₂But₃-2,4,6)

Guidance literature:: With NH₃; In hexane; react. BCl2(NHC6H2But3-2,4,6) with excess NH3(g) in n-C6H14 at 25°C for 3 h; filtration and crystn. at -30°C from concd. filtrate followed bysublimation; elem. anal.;
DOI:10.1039/c39840000662

Reference yield:

: 91915-27-4
BCl₂(NHC₆H₂But₃-2,4,6)

: 91915-30-9
(NH₃C₆H₂But₃-2,4,6)(BF₄)

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / hexane

2: diethyl ether

With NH₃; In diethyl ether; hexane;
DOI:10.1039/c39840000662